双(三氟甲基)二硫化物合成路线 (共 250 条)
反应条件
C6H5MgX
T=-78°C; other Grignard reagents, var. temperature; Product distributionMechanism;
参考文献
Munavalli, S.; Rossman, D. I.; Rohrbaugh, D. K.; Ferguson, C. P.
Journal of Fluorine Chemistry, 1993 , vol. 61, # 1.2 p. 147 - 153
参考文献
Haszeldine; Kidd
Journal of the Chemical Society, 1953 , p. 3871,3878
反应条件
in dichloromethane
1) -75 deg C, 2) 20 deg C, 50 min;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
in dichloromethane
-80 deg C to 20 deg C;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
chlorine
Irradiation.bei mehrtaegiger Bestrahlung mit UV-Licht;
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.2, page 157 - 193
反应条件
Irradiation (UV/VIS);
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.6, page 195 - 217
反应条件
fluoroether acid in acetonitrile-D3; acetonitrile
T=-50°C; 1 h; other temperatures, other exposition, other products; Product distribution;
参考文献
Dunkelberg, Oliver; Haas, Alois; Klapdor, Martin Frank; Mootz, Dietrich; Poll, Wolfgang; Appelman, Evan Hugh
Chemische Berichte, 1994 , vol. 127, # 10 p. 1871 - 1876
反应条件
Irradiation (UV/VIS); equimolar mixt., low yield;
参考文献
Zack; Shreeeve
Inorganic and Nuclear Chemistry Letters, 1974 , vol. 10, p. 619
反应条件
Irradiation (UV/VIS); equimolar mixt., low yield;
参考文献
Zack; Shreeeve
Inorganic and Nuclear Chemistry Letters, 1974 , vol. 10, p. 619
反应条件
byproducts: SF4; -196 to 0°C;
参考文献
Mir,Q.-C. et al.
Journal of the American Chemical Society, 1979 , vol. 101, p. 5949 - 5953