1,5-二苯基-3-甲基-1H-吡唑合成路线 (共 51 条)
反应条件
pyridine; potassium permanganate
参考文献
Finar; Simmonds
Journal of the Chemical Society, 1958 , p. 200,203
反应条件
anhydrous iron chloride in acetic acid
T=120°C; Reagent/catalystSolventTimeConcentration;
参考文献
Ananthnag, Guddekoppa S.; Adhikari, Adithya; Balakrishna, Maravanji S.
Catalysis Communications, 2014 , vol. 43, p. 240 - 243
反应条件
oxygen in 1,2-dichloro-benzene
T=130°C; 5 h;
参考文献
Yu, Jin; Kim, Ko Hoon; Moon, Hye Ran; Kim, Jae Nyoung
Bulletin of the Korean Chemical Society, 2014 , vol. 35, # 6 p. 1692 - 1696
反应条件
potassium tert-butylate in tert-butyl alcohol
9 h; Reflux; regioselective reaction;
参考文献
Jin, Weiwei; Yu, Haifeng; Yu, Zhengkun
Tetrahedron Letters, 2011 , vol. 52, # 44 p. 5884 - 5887
反应条件
{RuCl2(1-methyl-4-(1-methylethyl)benzene)}2; oxygen; sodium hydrogencarbonate in dimethyl sulfoxide
T=100°C; P=760.051 Torr; 5 h; Inert atmosphere; TemperatureTimeReagent/catalyst;
参考文献
Hu, Jiantao; Chen, Shi; Sun, Yonghui; Yang, Jing; Rao, Yu
Organic Letters, 2012 , vol. 14, # 19 p. 5030 - 5033,4
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane
T=100°C; Suzuki coupling; 16 h;
参考文献
Dvorak, Curt A.; Rudolph, Dale A.; Ma, Sandy; Carruthers, Nicholas I.
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 4188 - 4190
反应条件
1,4-diaza-bicyclo[2.2.2]octane; oxygen; copper diacetate in dimethyl sulfoxide
T=100°C; P=760.051 Torr; 12 h;
参考文献
Li, Xianwei; He, Li; Chen, Huoji; Wu, Wanqing; Jiang, Huanfeng
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3636 - 3646
反应条件
acetic acid in ethanol
T=20°C; 24 h;
参考文献
Alberola, Angel; Calvo Bleye, Luis; Gonzalez-Ortega, Alfonso; Sadaba, M.Luisa; Sanudo, M.Carme
Heterocycles, 2001 , vol. 55, # 2 p. 331 - 352
反应条件
{RuCl2(1-methyl-4-(1-methylethyl)benzene)}2; oxygen; sodium hydrogencarbonate in dimethyl sulfoxide
T=100°C; P=760.051 Torr; 0.666667 h; Inert atmosphere;
参考文献
Hu, Jiantao; Chen, Shi; Sun, Yonghui; Yang, Jing; Rao, Yu
Organic Letters, 2012 , vol. 14, # 19 p. 5030 - 5033,4
反应条件
sodium acetate in ethanol
Condensation; 3 h; Heating;
参考文献
Genin, Michael J.; Biles, Carolyn; Keiser, Barb J.; Poppe, Susan M.; Swaney, Steven M.; Tarpley, W. Gary; Yagi, Yoshihiko; Romero, Donna L.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 5 p. 1034 - 1040