4-甲基戊-4-烯-2-酮合成路线 (共 26 条)
反应条件
potassium hydroxide; diethyl ether
参考文献
Nasarow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1938 , p. 704
Chem. Zentralbl., 1939 , vol. 110, # II p. 3403
参考文献
Stross; Monger; Finch
Journal of the American Chemical Society, 1947 , vol. 69, p. 1627
反应条件
in pentane 90 h; Irradiation;
参考文献
Yang,N.C.; Thap,D.-M.
Tetrahedron Letters, 1966 , p. 3671 - 3675
反应条件
copper(l) iodide; lithium aluminium tetrahydride in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=-78°C; 60 h;
参考文献
Tsuda, Tetsuo; Fujii, Tomoyuki; Kawasaki, Kaoru; Saegusa, Takeo
Journal of the Chemical Society, Chemical Communications, 1980 , # 21 p. 1013 - 1014
反应条件
potassium hydroxide in tert-butyl alcohol
参考文献
Chapman,N.B. et al.
Journal of Organic Chemistry, 1970 , vol. 35, p. 917 - 923
反应条件
in tetrahydrofuran T=35°C; 3 h;
参考文献
Serebryakov, E. P.; Gamalevich, G. D.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 1740 - 1742
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 8 p. 1890 - 1892
参考文献
Chabalier,J. et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1967 , vol. 264, p. 1186 - 1188
反应条件
tetra-(n-butyl)ammonium iodide in N,N-dimethyl-formamide
T=0 - 10°C; electrolysis;
参考文献
d'Incan, Esther; Sibille, Soline; Perichon, Jacques; Moingeon, Marie-Odile; Chaussard, Jacques
Tetrahedron Letters, 1986 , vol. 27, # 35 p. 4175 - 4176
反应条件
phosphoric acid
T=140 - 145°C; 18 h;
参考文献
Serebryakov, E. P.; Gamalevich, G. D.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 1740 - 1742
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 8 p. 1890 - 1892
反应条件
diethyl ether; boron trifluoride
T=0°C; Destillation des Reaktionsprodukts;
参考文献
Hagemeyer
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 769