2,2,3,3,4,4,4-七氟丁醛水合物合成路线 (共 15 条)
反应条件
sulfuric acid; phosphorus pentoxide
参考文献
Journal of the American Chemical Society, , vol. 74, p. 5422,5425
Journal of the American Chemical Society, , vol. 76, p. 300
Journal of the American Chemical Society, , vol. 76, p. 4027
反应条件
tetrahydrofuran; nitrogen T=-80°C; Hydrolysis.bei anschliessenden Hydrolyse und Dehydratisierung des erhaltenen Heptafluorbutyraldehyd-hydrats mit hilfe von Phosphor(V)-oxid;
参考文献
Journal of the American Chemical Society, , vol. 75, p. 992
反应条件
tetrachloromethane; chlorine T=60°C; Irradiation.unter Belichtung;
参考文献
Journal of the American Chemical Society, , vol. 75, p. 1609
反应条件
iso-propylmagnesium bromide
参考文献
Journal of the American Chemical Society, , vol. 77, p. 917
反应条件
in tetrahydrofuran reaction at -80°C, 23 hours and at -30°C, 20 hours; distillation over P2O5;;
参考文献
Journal of the American Chemical Society, , vol. 75, p. 992
F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
T=690°C; P=3 - 4 Torr; 0.5 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2258 - 2267
参考文献
Journal of the American Chemical Society, , vol. 75, p. 1609
参考文献
McBee et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 86
参考文献
McBee et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1387,1390
反应条件
1: With water; titanium tetrachloride in dichloromethane T=-20 - 25°C; 16 h; 2: With potassium hydroxide; tetrabutylammomium bromide in dichloromethane T=25°C; 12 h;
参考文献
Bouillon, Jean-Philippe; Tinant, Bernard; Nuzillard, Jean-Marc; Portella, Charles
Synthesis, 2004 , # 5 p. 711 - 721