in benzene byproducts: Bu3SnCl; Irradiation (UV/VIS); mixt. of substrate and mercurial is irradiated in nitrogen-purged solvent in Pyrex tube with 350-nm Rayonet photoreactor for 24 h; GLC, (1)H-NMR, GCMS;
参考文献
Organometallics, , vol. 7, p. 696 - 702
→
反应条件
2-chloro-1,2-diphenyl-ethanone; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran T=60°C; 5 h;
参考文献
Zhao, Yingsheng; Wang, Haibo; Hou, Xiaohui; Hu, Yanhe; Lei, Aiwen; Zhang, Heng; Zhu, Lizheng
Journal of the American Chemical Society, 2006 , vol. 128, # 47 p. 15048 - 15049
1: (2-methyl-2-phenylpropyl)MgCl With zinc(II) chloride in tetrahydrofuran T=20°C; 2: 1-tributylstannyl-2-phenylacetylene With bis(dibenzylideneacetone)-palladium(0) in dichloromethane Further stages.;
