2-亚甲基丙烷-1,3-二基二乙酸酯合成路线 （共 21 条）
参考文献
Issidorides; Matar
Journal of the American Chemical Society, 1955 , vol. 77, p. 6382
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Lukes; Plesek
Collection of Czechoslovak Chemical Communications, 1956 , vol. 21, p. 1305,1308
Chemicke Listy, 1955 , vol. 49, p. 1826,1829
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Seu; Kho
Tetrahedron Letters, 1992 , vol. 33, # 46 p. 7015 - 7016
反应条件
1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 1 h / 80 °C
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C
2.2: 3 h / -78 °C
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参考文献
Sari, Ozkan; Hamada, Manabu; Roy, Vincent; Nolan, Steven P.; Agrofoglio, Luigi A.
Organic Letters, 2013 , vol. 15, # 17 p. 4390 - 4393
反应条件
sodium acetate
T=115 - 118°C; 3 h; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Gevorkyan; Arakelyan; Avakyan; Obosyan
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 2 p. 289 - 294
反应条件
triethylamine
Reflux;
参考文献
Espeel, Pieter E. R.; Piens, Kathleen; Callewaert, Nico; Van Der Eycken, Johan
Synlett, 2008 , # 15 p. 2321 - 2325
反应条件
in acetic acid
T=120°C; 1 h; reaction conditions (solvent, temperature, time and molar ratio) investigated; Product distribution;
参考文献
Chalova, O. B.; Chistoedova, G. B.; Kiladze, T. K.; Germash, E. V.; Kantor, E. A.; Rakhmankulov, D. L.
J. Appl. Chem. USSR (Engl. Transl.), 1988 , vol. 61, # 4 p. 934 - 937,853 - 855
参考文献
Nerdel et al.
Chemische Berichte, 1958 , vol. 91, p. 938,941
参考文献
Nerdel et al.
Chemische Berichte, 1958 , vol. 91, p. 938,941
参考文献
Chalova, O. B.; Chistoedova, G. B.; Kiladze, T. K.; Germash, E. V.; Kantor, E. A.; Rakhmankulov, D. L.
J. Appl. Chem. USSR (Engl. Transl.), 1988 , vol. 61, # 4 p. 934 - 937,853 - 855
参考文献
Nerdel et al.
Chemische Berichte, 1958 , vol. 91, p. 938,941
参考文献
Nerdel et al.
Chemische Berichte, 1958 , vol. 91, p. 938,941
