3,4-二氢-1,2-萘二甲酸酐合成路线 （共 10 条）
反应条件
bromine; acetic acid T=100°C; im Rohr;
参考文献
Hershberg; Fieser
Organic Syntheses, 1938 , vol. 18, p. 59
Organic Syntheses, 1943 , vol. Coll. Vol. II, p. 423
Full Text Show Details
Fieser; Hershberg
Journal of the American Chemical Society, 1935 , vol. 57, p. 1851,1853
参考文献
v. Auwers; Moeller
Journal fuer Praktische Chemie (Leipzig), 1925 , vol. <2> 109, p. 126,139
反应条件
1,3-bis-(diphenylphosphino)propane; acetic acid; triethylamine; palladium dichloride
T=120°C; P=7600.51 Torr; 3 h; Autoclave;
参考文献
Bae, Yeon Kyu; Cho, Chan Sik
Synlett, 2013 , vol. 24, # 14 art. no. ST-2013-U0446-L, p. 1848 - 1850
反应条件
1,3-bis-(diphenylphosphino)propane; acetic acid; triethylamine; palladium dichloride
T=120°C; P=7600.51 Torr; 3 h; Autoclave;
参考文献
Bae, Yeon Kyu; Cho, Chan Sik
Synlett, 2013 , vol. 24, # 14 art. no. ST-2013-U0446-L, p. 1848 - 1850
反应条件
sulfuric acid
T=20°C;
参考文献
Hershberg; Fieser
Organic Syntheses, 1938 , vol. 18, p. 25
Coll. Vol., 1943 , vol. II, p. 195
Full Text Show Details
Fieser; Hershberg
Journal of the American Chemical Society, 1935 , vol. 57, p. 1851,1853
Full Text Show Details
v. Auwers; Moeller
Journal fuer Praktische Chemie (Leipzig), 1925 , vol. <2> 109, p. 126,139
反应条件
1: phosphorus tribromide
2: sodium chlorite; dihydrogen peroxide
3: palladium dichloride; 1,3-bis-(diphenylphosphino)propane; triethylamine; acetic acid / 3 h / 120 °C / 7600.51 Torr / |Autoclave
View Scheme
参考文献
Bae, Yeon Kyu; Cho, Chan Sik
Synlett, 2013 , vol. 24, # 14 art. no. ST-2013-U0446-L, p. 1848 - 1850
反应条件
1: phosphorus tribromide
2: sodium chlorite; dihydrogen peroxide
3: palladium dichloride; 1,3-bis-(diphenylphosphino)propane; triethylamine; acetic acid / 3 h / 120 °C / 7600.51 Torr / |Autoclave
View Scheme
参考文献
Bae, Yeon Kyu; Cho, Chan Sik
Synlett, 2013 , vol. 24, # 14 art. no. ST-2013-U0446-L, p. 1848 - 1850
反应条件
1: sodium chlorite; dihydrogen peroxide
2: palladium dichloride; 1,3-bis-(diphenylphosphino)propane; triethylamine; acetic acid / 3 h / 120 °C / 7600.51 Torr / |Autoclave
View Scheme
参考文献
Bae, Yeon Kyu; Cho, Chan Sik
Synlett, 2013 , vol. 24, # 14 art. no. ST-2013-U0446-L, p. 1848 - 1850
参考文献
v. Auwers; Moeller
Journal fuer Praktische Chemie (Leipzig), 1925 , vol. <2> 109, p. 126,139
反应条件
palladium on activated charcoal in methanol; acetic acid
T=120°C; 48 h;
参考文献
Mizuno, Masahiro; Yamano, Mitsuhisa
Heterocycles, 2006 , vol. 67, # 2 p. 807 - 814
