1-(溴甲基磺酰基)-4-甲基苯合成路线 （共 24 条）
参考文献
Synthesis, , # 13 p. 2094 - 2098
反应条件
n-butyllithium; methanesulfonyl chloride; triethylamine (one pot); 1.) THF, -30 deg C, 1 h, 2.) THF, -30 deg C, 1 h, 3.) THF, -30 deg C to RT, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Makosza, Mieczyslaw; Podraza, Renata; Bialecki, Maciej
Gazzetta Chimica Italiana, 1995 , vol. 125, # 12 p. 601 - 604
参考文献
Ziegler; Connor
Journal of the American Chemical Society, 1940 , vol. 62, p. 2598
参考文献
Ziegler; Connor
Journal of the American Chemical Society, 1940 , vol. 62, p. 2598
参考文献
Ziegler; Connor
Journal of the American Chemical Society, 1940 , vol. 62, p. 2598
参考文献
Xu, Wei Ming; Tang, E; Huang, Xian
Synthesis, 2004 , # 13 p. 2094 - 2098
反应条件
in various solvent(s)
T=80°C; 4 h;
参考文献
Sukata
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 2 p. 613 - 614
反应条件
sodium hydroxide
T=20°C; 0.5 h;
参考文献
Suryakiran; Prabhakar; Srikanth Reddy; Chinni Mahesh; Rajesh; Venkateswarlu
Tetrahedron Letters, 2007 , vol. 48, # 5 p. 877 - 881
反应条件
sodium hydroxide
T=20°C; 0.5 h;
参考文献
Suryakiran; Prabhakar; Srikanth Reddy; Chinni Mahesh; Rajesh; Venkateswarlu
Tetrahedron Letters, 2007 , vol. 48, # 5 p. 877 - 881
反应条件
1: moist tetrachloromethane; bromine
2: sodium ethylate
View Scheme
参考文献
Ziegler; Connor
Journal of the American Chemical Society, 1940 , vol. 62, p. 1051
