8-甲氧基-9-硼杂双环[3.3.1]壬烷合成路线 （共 45 条）
反应条件
in diethyl ether T=25°C; 24 h;
参考文献
Molander, Gary A.; Singaram, Bakthan; Brown, Herbert C.
Journal of Organic Chemistry, 1984 , vol. 49, # 25 p. 5024 - 5025
参考文献
Gmelin Handbook: B: B-Verb.14, 5.6, page 212 - 224
反应条件
in toluene T=-78 - 20°C; 2 h; Inert atmosphere;
参考文献
Takeuchi, Katsuhiko; Ichinohe, Masaaki; Sekiguchi, Akira
Organometallics, 2011 , vol. 30, # 7 p. 2044 - 2050
反应条件
in benzene-d6 T=20°C; P=760.051 Torr; 8 h;
参考文献
Chakraborty, Sumit; Zhang, Jie; Patel, Yogi J.; Krause, Jeanette A.; Guan, Hairong
Inorganic Chemistry, 2013 , vol. 52, # 1 p. 37 - 47
反应条件
[(N((CH2)2NHPiPr2)2((CH2)2NP(C7H6O)iPr2))Ru]BPh4 in dichloromethane-d2 T=50°C; P=760.051 Torr; Sealed tube; Catalytic behavior; TimeConcentration;
参考文献
Chakraborty, Sumit; Zhang, Jie; Patel, Yogi J.; Krause, Jeanette A.; Guan, Hairong
Inorganic Chemistry, 2013 , vol. 52, # 1 p. 37 - 47
反应条件
1: deuterated toluene / 22 °C 2: (tBuPOCOP)NiH / benzene-d6 / 1 h / 20 °C / 760.05 Torr / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Chakraborty, Sumit; Zhang, Jie; Patel, Yogi J.; Krause, Jeanette A.; Guan, Hairong
Inorganic Chemistry, 2013 , vol. 52, # 1 p. 37 - 47
反应条件
in diethyl ether T=25°C; 24 h;
参考文献
Molander, Gary A.; Singaram, Bakthan; Brown, Herbert C.
Journal of Organic Chemistry, 1984 , vol. 49, # 25 p. 5024 - 5025
反应条件
in diethyl ether T=25°C; 24 h;
参考文献
Molander, Gary A.; Singaram, Bakthan; Brown, Herbert C.
Journal of Organic Chemistry, 1984 , vol. 49, # 25 p. 5024 - 5025
反应条件
in diethyl ether T=25°C; 24 h;
参考文献
Molander, Gary A.; Singaram, Bakthan; Brown, Herbert C.
Journal of Organic Chemistry, 1984 , vol. 49, # 25 p. 5024 - 5025
反应条件
in toluene Ar atmosphere; refluxing (24 h), slow cooling (-78°C); washing (toluene, -78°C), drying (vac.) and elem. anal. of dithio-compd., boryl compds. from the mother liquor;
参考文献
Koester, Roland; Kucznierz, Ralf; Seidel, Guenter; Betz, Peter
Chemische Berichte, 1992 , vol. 125, # 5 p. 1023 - 1032
