二乙基(苯基硫代甲基)磷酸酯合成路线 （共 43 条）
反应条件
in toluene 1 h; Heating;
参考文献
Balczewski,Piotr
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 104, # 14 p. 113 - 122
反应条件
1: triethylamine / dichloromethane / 3.5 h / 20 °C 2: caesium carbonate / N,N-dimethyl-formamide / 20 °C View Scheme
参考文献
Woo, Seo Yeon; Kim, Ji Hyun; Moon, Mi Kyeong; Han, Se-Hee; Yeon, Seul Ki; Choi, Ji Won; Jang, Bo Ko; Song, Hyo Jung; Kang, Yong Gu; Kim, Jin Woo; Lee, Jaeick; Kim, Dong Jin; Hwang, Onyou; Park, Ki Duk
Journal of Medicinal Chemistry, 2014 , vol. 57, # 4 p. 1473 - 1487
参考文献
Arbusow; Bogonoszewa
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2356,2358;engl.Ausg.S.2415,2417
反应条件
(i) NaH, THF, (ii) /BRN= 1617369/; Multistep reaction;
参考文献
Coutrot,P. et al.
Synthesis, 1976 , p. 107 - 108
反应条件
1.) C4H9Li 1.) toluene, -20 deg C 2.) 110 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Flitsch, Wilhelm; Rosche, Juergen; Lubisch, , Wilfried
Liebigs Annalen der Chemie, 1987 , p. 661 - 664
参考文献
Cao, Yi; Hidaka, Asami; Tajima, Toshiki; Fuchigami, Toshio
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9614 - 9617
反应条件
1: n-BuLi / 1.) THF, -78 deg C, 2.) THF, from -78 to 25 deg C 2: 76 percent / n-Bu3SnH, AIBN / toluene / 1 h / Heating View Scheme
参考文献
Balczewski,Piotr
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 104, # 14 p. 113 - 122
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene 1 h; Heating;
参考文献
Balczewski,Piotr
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 104, # 14 p. 113 - 122
反应条件
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h 2.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C 2.2: 1 h / -78 - 20 °C View Scheme
参考文献
Woo, Seo Yeon; Kim, Ji Hyun; Moon, Mi Kyeong; Han, Se-Hee; Yeon, Seul Ki; Choi, Ji Won; Jang, Bo Ko; Song, Hyo Jung; Kang, Yong Gu; Kim, Jin Woo; Lee, Jaeick; Kim, Dong Jin; Hwang, Onyou; Park, Ki Duk
Journal of Medicinal Chemistry, 2014 , vol. 57, # 4 p. 1473 - 1487
反应条件
1.1: Oxone 2.1: LHMDS / tetrahydrofuran / 0.33 h / -78 °C 2.2: 100 percent / tetrahydrofuran / 2 h / -78 - -40 °C View Scheme
参考文献
Yamamoto, Iwao; Sakai, Toshito; Yamamoto, Sigeto; Ohta, Kazuchika; Matsuzaki, Kei
Synthesis, 1985 , # 6/7 p. 676 - 677
