1,1,1-三氟-2-丁酮合成路线 (共 16 条)
反应条件
1: in diethyl ether T=-78°C; 1 h; 2: With hydrogenchloride in diethyl ether; water
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: WO2008/143332 A1, 2008 ;
Location in patent: Page/Page column 141 ;
反应条件
tetraethylplumbane T=90°C; Oxidation; P=51714.8 Torr; 24 h; Further byproducts given;
参考文献
Hogan, Terrence; Sen, Ayusman
Journal of the American Chemical Society, 1997 , vol. 119, # 11 p. 2642 - 2646
反应条件
ethene; dihydrogen peroxide in water T=75 - 80°C; Oxidation; P=51714.8 Torr; 24 h; Further byproducts given;
参考文献
Hogan, Terrence; Sen, Ayusman
Journal of the American Chemical Society, 1997 , vol. 119, # 11 p. 2642 - 2646
反应条件
sulfuric acid; acetic acid
参考文献
Burdon,J.; McLoughlin,V.C.R.
Tetrahedron, 1964 , vol. 20, p. 2162 - 2166
反应条件
sodium dichromate; sulfuric acid; water
参考文献
Sykes et al.
Journal of the Chemical Society, 1956 , p. 835,839
反应条件
magnesium 1.) Et2O, 2.) r.t, 30 min; Multistep reaction;
参考文献
Xiao, Ling; Yamazaki, Takashi; Kitazume, Tomoya; Yonezawa, Tetsuo; Sakamoto, Yoshitake; Nogawa, Kouji
Journal of Fluorine Chemistry, 1997 , vol. 84, # 1 p. 19 - 23
反应条件
anhydrous butyl ether
参考文献
Haszeldine
Journal of the Chemical Society, 1954 , p. 1273,1278
反应条件
anhydrous butyl ether
参考文献
Sykes et al.
Journal of the Chemical Society, 1956 , p. 835,839
参考文献
Hudlicky,M.
Collection of Czechoslovak Chemical Communications, 1961 , vol. 26, p. 3140 - 3146
参考文献
Johnson, Cris E.; Sannes, Kristin A.; Brauman, John I.
Journal of Physical Chemistry, 1996 , vol. 100, # 21 p. 8827 - 8835