methyllithium 550 kg Cr2O3, 225 kg Al powder, 50-55 kg KClO3 and 50-55 kg lime put into Fe covering cylinder;
参考文献
Kurnakov, N. N.; Kornilov, I. I.; Boky, G. B.
Doklady Akademii Nauk SSSR, 1938 , vol. 18, p. 583 - 584
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Gmelin Handbook: Cr: MVol.A1, 5.1.1, page 213 - 217
H2SO4/(COOH)2 mixt. in not given sample oxidn. in sulfuric acid/oxalic acid mixt., according to E. Brauer, Ed., Handbook of Preparative Inorganic Chemistry, Vol. 1, p. 301; Academic Press, New York, 1963; storing in perchloric acid at 4°C;
参考文献
Herschkowitsch
Z. Anorg. Chem., 1922 , vol. 125, p. 177 - 177
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Gmelin Handbook: Cl: MVol., 85, page 234 - 236
oxalic acid in neat (no solvent) H2O removing (P2O5), vac. distillation; IR;
参考文献
Wallington, Timothy J.; Cox, Richard A.
Journal of the Chemical Society, Faraday Transactions 2: Molecular and Chemical Physics, 1986 , vol. 82, p. 275 - 290
iron(III) chloride in neat (no solvent) heating a moistened mixture of FeCl3 and KClO3 up to 100 °C;;
参考文献
Martens
Ann. Chim. Phys., 1836 , vol. 61, p. 307 - 307
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Martens
Journal fuer Praktische Chemie (Leipzig), 1836 , vol. 8, p. 272 - 272
