in neat (no solvent) byproducts: KCl; High Pressure; molar ratio 1/1, platinum crucible, 20 kbar, 1400°C. 20 min; cooling to 800°C within 60 min; quenching to normal conditions; in microcrystalline KCl matrix;
in water mixing components solns. (small amount of NH3OH-salt), water removal (distn.) to dryness; no isolation in pure state; IR spectroscopy;
参考文献
Titova, K. V.; Kolmakova, E. I.; Rosolovskii, V. Ya.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1978 , vol. 23, p. 634 - 636
Zhurnal Neorganicheskoi Khimii, 1978 , vol. 23, p. 1146 - 1149
