甲基2-吡啶羧酸酯1-氧化物合成路线 （共 13 条）
反应条件
1: With ammonium formate; 10percent palladium on carbon in methanol T=20°C; 16 h; 2: With hydrogenchloride in methanol Further stages.;
参考文献
Zacharie; Moreau; Dockendorff
Journal of Organic Chemistry, 2001 , vol. 66, # 15 p. 5264 - 5265
反应条件
trichlorophosphate T=80°C; 17 h; Yield given. Yields of byproduct given;
参考文献
Heerding, Dirk; Saunders, David
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 6 p. 455 - 460
反应条件
trichlorophosphate T=80°C; 17 h; Yield given. Yields of byproduct given;
参考文献
Heerding, Dirk; Saunders, David
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 6 p. 455 - 460
反应条件
1: Ts2O / various solvent(s); CH2Cl2 / 0.25 h 2: TFA / various solvent(s); CH2Cl2 / 70 °C View Scheme
参考文献
Yin, Jingjun; Xiang, Bangping; Huffman, Mark A.; Raab, Conrad E.; Davies, Ian W.
Journal of Organic Chemistry, 2007 , vol. 72, # 12 p. 4554 - 4557
反应条件
copper(l) iodide; zinc in ethanol T=55 - 60°C; 1.5 h;
参考文献
Singh, Sunil Kumar; Srinivasa Reddy; Mangle, Mangesh; Ravi Ganesh
Tetrahedron, 2007 , vol. 63, # 1 p. 126 - 130
反应条件
in acetonitrile T=81°C; 4 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 44, # 2 p. 487 - 489
反应条件
diazomethyl-trimethyl-silane in hexane
T=0°C;
参考文献
Yang, Kai; Qiu, Yatao; Li, Zheng; Wang, Zhaoyang; Jiang, Sheng
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3151 - 3159
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
48 h; Ambient temperature;
参考文献
Heerding, Dirk; Saunders, David
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 6 p. 455 - 460
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.17 h / 0 °C
2: thionyl chloride / 0 °C / Reflux
View Scheme
参考文献
Yang, Kai; Qiu, Yatao; Li, Zheng; Wang, Zhaoyang; Jiang, Sheng
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3151 - 3159
反应条件
1: aqueous H2O2; acetic acid
2: Einleiten von HCl
View Scheme
参考文献
Krause; Langenbeck
Chemische Berichte, 1959 , vol. 92, p. 155,158
