2,6-二叔丁基-4-甲基吡啶合成路线 （共 19 条）
反应条件
in tetrahydrofuran 4 h; Heating;
参考文献
Bates, Robert B.; Gordon, Bernard; Keller, Philip C.; Rund, John V.; Mills, Nancy S.,
Journal of Organic Chemistry, 1980 , vol. 45, # 1 p. 168 - 169
反应条件
1: tin (IV)-chloride; aqueous perchloric acid / Hydrolysis 2: aqueous ammonia View Scheme
参考文献
Balaban; Nenitzescu
Justus Liebigs Annalen der Chemie, 1959 , vol. 625, p. 74,83
反应条件
ammonium hydroxide; methanesulfonic acid 1.) 100 deg C, 1 h; 2.) 45 min.; Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rajoharison, Harivelo G.; Roussel, Christian
Bulletin de la Societe Chimique de France, 1986 , # 2 p. 307 - 313
反应条件
trifluoroacetic anhydride in dichloromethane; water
参考文献
Abbott Laboratories
Patent: US2005/245531 A1, 2005 ;
US 20050245531 A1
反应条件
H2O in chloroform-d1 water was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and mixt. was allowed to stand at room temp. for 33 h; detn. by NMR;
参考文献
Organometallics, , vol. 19, # 12 p. 2258 - 2263
反应条件
in chloroform-d1 alcohol was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and allowed to react at 23°C for 4-7 h; detn. by NMR;
参考文献
Organometallics, , vol. 19, # 12 p. 2258 - 2263
反应条件
H2O in chloroform-d1 water was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and mixt. was allowed to stand at room temp. for 33 h; detn. by NMR;
参考文献
Organometallics, , vol. 19, # 12 p. 2258 - 2263
反应条件
in chloroform-d1 alcohol was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and allowed to react at 23°C for 4-7 h; detn. by NMR;
参考文献
Organometallics, , vol. 19, # 12 p. 2258 - 2263
反应条件
in chloroform-d1 Kinetics; alcohol was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and allowed to react at 23°C for 4-7 h; detn. by NMR;
参考文献
Organometallics, , vol. 19, # 12 p. 2258 - 2263
反应条件
in chloroform-d1 alcohol was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and allowed to react at 23°C for 4-7 h; detn. by NMR;
参考文献
Organometallics, , vol. 19, # 12 p. 2258 - 2263
