2,6-二叔丁基-4-甲基吡啶合成路线 （共 19 条）
反应条件
in chloroform-d1 alcohol was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and allowed to react at 23°C for 4-7 h; detn. by NMR;
参考文献
Organometallics, , vol. 19, # 12 p. 2258 - 2263
反应条件
trifluoromethylsulfonic anhydride in dichloromethane; pentane
参考文献
Merck and Co., Inc.
Patent: US6455532 B1, 2002 ;
US 6455532 B1
反应条件
in dichloromethane; pentane
参考文献
Merck and Co., Inc.
Patent: US6610692 B1, 2003 ;
US 6610692 B1
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 5 h; Heating;
参考文献
Mobinikhaledi; Foroughifar
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 2 p. 405 - 412
反应条件
in chloroform-d1 alcohol was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and allowed to react at 23°C for 4-7 h; detn. by NMR;
参考文献
Organometallics, , vol. 19, # 12 p. 2258 - 2263
反应条件
in chloroform-d1 alcohol was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and allowed to react at 23°C for 4-7 h; detn. by NMR;
参考文献
Organometallics, , vol. 19, # 12 p. 2258 - 2263
反应条件
trifluorormethanesulfonic acid in dichloromethane T=25°C;
参考文献
EP1371646 A1, ;
Page 40 ;
反应条件
sodium hydrogencarbonate in dichloromethane; ethyl acetate
参考文献
O'NEIL, Jennifer; BENITA, Yair; MARINE, Shane; HAINES, Brian
Patent: US2012/289481 A1, 2012 ;
反应条件
in chloroform-d1
Kinetics; alcohol was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and allowed to react at 23°C for 4-7 h; detn. by NMR;
参考文献
Matano, Yoshihiro
Organometallics, 2000 , vol. 19, # 12 p. 2258 - 2263
