1-甲氧基-4-((e)-3-苯基烯丙氧基)-苯合成路线 （共 9 条）
反应条件
1: 4-methoxy-phenol With sodium hydride in N,N-dimethyl-formamide
T=20°C; 0.166667 h;
2: trans-cinnamyl acetate With tetrakis(triethylphosphite)nickel(O) in tetrahydrofuran; N,N-dimethyl-formamide
T=50°C; 20 h; Further stages.;
参考文献
Yatsumonji, Yasutaka; Ishida, Yusuke; Tsubouchi, Akira; Takeda, Takeshi
Organic Letters, 2007 , vol. 9, # 22 p. 4603 - 4606
反应条件
1: (E)-(3-chloro-1-propenyl)benzene With bis[(4S,5R)-diphenyl-4,5-dihydrooxazole]methane; potassium carbonate; [Cp*Ru(CNCH3)3]+PF6- in acetone
T=0°C; 0.25 h;
2: 4-methoxy-phenol in acetone
T=0°C; 40 h;
参考文献
Mbaye, Mbaye D.; Renaud, Jean-Luc; Demerseman, Bernard; Bruneau, Christian
Chemical Communications, 2004 , # 16 p. 1870 - 1871
反应条件
potassium carbonate in acetone
参考文献
White,W.N.; Norcross,B.E.
Journal of the American Chemical Society, 1961 , vol. 83, p. 1968 - 1974
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Zahl,G. et al.
Justus Liebigs Annalen der Chemie, 1975 , p. 1733 - 1743
反应条件
dichloro(cycloocta-1,5-diene)palladium(II) in N,N-dimethyl acetamide
T=100°C; Heck Reaction; 16 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Wei; Zhou, Rong; Jiang, Zhi-Jie; Wang, Kun; Fu, Hai-Yan; Zheng, Xue-Li; Chen, Hua; Li, Rui-Xiang
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 616 - 622
反应条件
dichloro(cycloocta-1,5-diene)palladium(II) in N,N-dimethyl acetamide
T=110°C; Heck Reaction; 24 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Wei; Zhou, Rong; Jiang, Zhi-Jie; Wang, Kun; Fu, Hai-Yan; Zheng, Xue-Li; Chen, Hua; Li, Rui-Xiang
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 616 - 622
反应条件
potassium carbonate; (.eta.5-pentamethylcyclopentadienyl)(methyl diphenylphosphinite)bis(acetonitrile)ruthenium(II) PF6 in dichloromethane
T=20°C; 16 h; Title compound not separated from byproducts;
参考文献
Demerseman, Bernard; Renaud, Jean-Luc; Toupet, Loic; Hubert, Claudie; Bruneau, Christian
European Journal of Inorganic Chemistry, 2006 , # 7 p. 1371 - 1380
反应条件
tetrakis(triphenylphosphine) palladium(0); benzoic acid in 1,4-dioxane
T=100°C;
参考文献
Zhang, Weijiang; Haight, Anthony R.; Hsu, Margaret C.
Tetrahedron Letters, 2002 , vol. 43, # 37 p. 6575 - 6578
反应条件
1: potassium phosphate; tetrabutylammomium bromide / N,N-dimethyl acetamide / 4 h / 100 °C / |Inert atmosphere; |Schlenk technique
2: dichloro(cycloocta-1,5-diene)palladium(II) / N,N-dimethyl acetamide / 16 h / 100 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Wang, Wei; Zhou, Rong; Jiang, Zhi-Jie; Wang, Kun; Fu, Hai-Yan; Zheng, Xue-Li; Chen, Hua; Li, Rui-Xiang
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 616 - 622
反应条件
(Rearrangement)
T=180°C; Rate constant;
参考文献
Zahl,G. et al.
Justus Liebigs Annalen der Chemie, 1975 , p. 1733 - 1743
