in further solvent(s) to suspn. of Os complex in tetraglyme transferred in vac. CF3COOH (molar ratio 1:1), mixt. stirred at room temp. for 2 h, 2 equiv FSO3C2H5 distd. into react. vessel, mixt. stirred at room temp. for 5 min; mixt. of product and CF3COOCH3 distd. into -196°C cold trap, redistd. into -56°C trap, fractionated on vac. line (in -23°Ctrap);
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in trifluoroacetic acid 0 deg C, 30 min, then reflux 70 h; Title compound not separated from byproducts;
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