2-溴-3,3,3-三氟乙酸丙酯合成路线 （共 9 条）
反应条件
sodium hydroxide in water T=100°C; Title compound not separated from byproducts.;
参考文献
Ramachandran, P. Veeraraghavan; Padiya, Kamlesh J.
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1255 - 1259
反应条件
sulfuric acid; water 4 h; Heating / reflux;
参考文献
Ramachandran, P. V.; Padiya, Kamlesh J.; Mereddy, Venkatram R.
Patent: US2007/282137 A1, 2007 ;
Location in patent: Page/Page column 2 ;
反应条件
sulfuric acid 3 h; Heating;
参考文献
Ramachandran, P. Veeraraghavan; Padiya, Kamlesh J.
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1255 - 1259
反应条件
sodium hydroxide in water T=100°C; Title compound not separated from byproducts.;
参考文献
Ramachandran, P. Veeraraghavan; Padiya, Kamlesh J.
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1255 - 1259
参考文献
Knunyants,I.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1961 , p. 77 - 80
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , p. 88 - 93
反应条件
1: 1,1,2-trifluoro-propene With sulfuric acid; sulfur trioxide; bromine
T=12 - 22°C; 1 h;
2: acetic acid T=100°C; 1 h;
参考文献
Ramachandran, P. V.; Padiya, Kamlesh J.; Mereddy, Venkatram R.
Patent: US2007/282137 A1, 2007 ;
Location in patent: Page/Page column 2 ;
反应条件
bromine; silver(I) acetate
1 h;
参考文献
Ramachandran, P. Veeraraghavan; Padiya, Kamlesh J.
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1255 - 1259
反应条件
N-bromosuccinmide; sulfuric acid
T=65 - 70°C; 11 h; Title compound not separated from byproducts;
参考文献
Lermontov, S. A.; Kuryleva, N. V.; Velikokhat'ko, T. N.
Russian Chemical Bulletin, 2002 , vol. 51, # 3 p. 550 - 551
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2002 , # 3 p. 508 - 509
参考文献
Ramachandran, P. Veeraraghavan; Padiya, Kamlesh J.
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1255 - 1259
