1,1,2-三氟-1-丁烯合成路线 （共 6 条）
反应条件
lithium chloride in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8)
T=20°C; P=2660.18 Torr; 18 h; Inert atmosphere;
参考文献
Ohashi, Masato; Kamura, Ryohei; Doi, Ryohei; Ogoshi, Sensuke
Chemistry Letters, 2013 , vol. 42, # 8 p. 933 - 935
反应条件
lithium iodide in hexane
T=60°C; P=2660.18 Torr; 24 h; Inert atmosphere; SolventReagent/catalystTime;
参考文献
Ohashi, Masato; Kamura, Ryohei; Doi, Ryohei; Ogoshi, Sensuke
Chemistry Letters, 2013 , vol. 42, # 8 p. 933 - 935
反应条件
tri-tert-butyl phosphine; Pd2(dba)3*(benzene) in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8); hexane
T=20°C; P=2660.18 Torr; 4 h;
参考文献
Ohashi, Masato; Kamura, Ryohei; Doi, Ryohei; Ogoshi, Sensuke
Chemistry Letters, 2013 , vol. 42, # 8 p. 933 - 935
反应条件
lithium iodide in acetonitrile-D3
T=20°C; 0.5 h; Inert atmosphere;
参考文献
Ohashi, Masato; Kamura, Ryohei; Doi, Ryohei; Ogoshi, Sensuke
Chemistry Letters, 2013 , vol. 42, # 8 p. 933 - 935
反应条件
in hexane; acetonitrile-D3
T=60°C; P=2660.18 Torr; 24 h; Inert atmosphere;
参考文献
Ohashi, Masato; Kamura, Ryohei; Doi, Ryohei; Ogoshi, Sensuke
Chemistry Letters, 2013 , vol. 42, # 8 p. 933 - 935
反应条件
diethyl ether
T=-80°C;
参考文献
Dixon
Journal of Organic Chemistry, 1956 , vol. 21, p. 400,402
