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乙二醇
甲醛
63148-62-9
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二甲基亚砜
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
38384-58-6
合成路线
（共 13 条）
64-17-5
乙醇
+
501-65-5
二苯基乙炔
→
反应条件
38384-58-6
+
54444-14-3
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-30°C; 24 h; Title compound not separated from byproducts.;
参考文献
Ochiai, Masahito; Yoshimura, Akira; Mori, Takeshi; Nishi, Yoshio; Hirobe, Masaya
Journal of the American Chemical Society, 2008 , vol. 130, # 12 p. 3742 - 3743
109431-70-1
+
98-80-6
苯硼酸
→
反应条件
38384-58-6
反应条件
PPh3 gold(I) chloro complex; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in water; acetonitrile T=80°C; 0.5 h; Inert atmosphere;
参考文献
Zhang, Guozhu; Peng, Yu; Cui, Li; Zhang, Liming
Angewandte Chemie, International Edition, 2009 , vol. 48, # 17 p. 3112 - 3115
673-32-5
1-苯基-1-丙炔
+
201230-82-2
+
98-80-6
苯硼酸
→
反应条件
14182-01-5
+
38384-58-6
反应条件
tetrakis-(ethylene)-μ,μ'-dichlorodirhodium(I); trifluoroacetic acid in methanol; water T=80°C; P=3800.26 Torr; 16 h; Autoclave; regioselective reaction;
参考文献
Ku, Melih; Artok, Oezge Aksin; Ziyanak, Firat; Artok, Levent
Synlett, 2008 , # 17 p. 2587 - 2592
673-32-5
1-苯基-1-丙炔
+
98-88-4
苯甲酰氯
→
反应条件
38384-58-6
反应条件
1: 1-phenyl-1-propyne With bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride in tetrahydrofuran T=25°C; 0.5 h; Inert atmosphere; 2: benzoyl chloride With copper(l) iodide in benzene T=80°C; Stille cross-coupling; 10 h;
参考文献
Li, Jianying; Yu, Yan; Hao, Wenyan; Cai, Mingzhong
Journal of Chemical Research, 2010 , # 10 p. 559 - 561
→
反应条件
38384-58-6
反应条件
2,6-di-tert-butyl-pyridine; copper(l) chloride in dichloromethane T=50°C; Meyer-Schuster Rearrangement; Inert atmosphereSealed tube; Reagent/catalystTemperature;
参考文献
Collins, Beatrice S. L.; Suero, Marcos G.; Gaunt, Matthew J.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 22 p. 5799 - 5802
119-53-9
安息香
→
反应条件
38384-58-6
反应条件
1: 97 percent / 10percent sodium hydroxide / dimethylsulfoxide; H2O / 12 h / 25 °C 2: formic acid / 4 h / Heating View Scheme
参考文献
Padwa, Albert; Cohen, Leslie A.; Gingrich, Henry L.
Journal of the American Chemical Society, 1984 , vol. 106, # 4 p. 1065 - 1073
27739-61-3
→
反应条件
38384-58-6
+
54444-14-3
反应条件
in formic acid 4 h; Heating; Yield given. Yields of byproduct given;
参考文献
Padwa, Albert; Cohen, Leslie A.; Gingrich, Henry L.
Journal of the American Chemical Society, 1984 , vol. 106, # 4 p. 1065 - 1073
673-32-5
1-苯基-1-丙炔
+
100-51-6
苯甲醇
→
反应条件
38384-58-6
+
54444-14-3
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; tri-n-octyl phosphine in toluene T=120°C; 15 h; Inert atmospherePressure tube; optical yield given as percent de;
参考文献
Hatanaka, Shintaro; Obora, Yasushi; Ishii, Yasutaka
Chemistry - A European Journal, 2010 , vol. 16, # 6 p. 1883 - 1888
36854-57-6
2-苯基丁酰氯
+
98-88-4
苯甲酰氯
→
反应条件
38384-58-6
+
54444-14-3
反应条件
(Ph3P)2Pd(Ph)(Br) in tetrahydrofuran T=140°C; 5 h; cross-condensation reactions with other aroyl chlorides; MechanismProduct distribution;
参考文献
Mitsudo, Take-aki; Kadokura, Mamoru; Watanabe, Yoshihisa
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3186 - 3192
591-50-4
碘苯
+
201230-82-2
+
17336-66-2
1-丙基酰苯甲苯磺酰腙
→
反应条件
16282-16-9
2-苯基丁酰苯
+
38384-58-6
+
54444-14-3
反应条件
triethylsilane; tetrakis(triphenylphosphine) palladium(0); isopropylamine; lithium tert-butylate in 1,4-dioxane T=70°C; 15 h; optical yield given as percent de;
参考文献
Zhang, Zhenhua; Liu, Yiyang; Gong, Mingxing; Zhao, Xiaokun; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2010 , vol. 49, # 6 p. 1139 - 1142
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