反应条件
H2O in tetrahydrofuran
a Ge-contg.-compd. was added to a mixt. of tri-tert-butylcyclopropenyl tetrafluoroborate (15.5 mmol) and THF at 0°C; after stirring at 0°C for 1 h, the mixt. was hydrolyzed with water; org. layer was sepd., aq. layer was extd. with hexane; org. layer and exts. were combined, washed with H2O and brine, dried, filtered; filtrate was concd. under reduced pressure; residue was chromd. on silica gel (hexane as eluent), concd.; elem. anal.;
参考文献
Tsutsui, Shinobu; Tanaka, Hiromasa; Kwon, Eunsang; Matsumoto, Shigeki; Sakamoto, Kenkichi
Journal of Organometallic Chemistry, 2006 , vol. 691, # 4 p. 595 - 603
