3,4,5-三甲氧基苄醇合成路线 （共 102 条）
反应条件
sodium tetrahydroborate; lithium chloride in diethylene glycol dimethyl ether T=162°C; 5 h;
参考文献
Zhu, Hua-Jie; Pittman Jr., Charles U.
Synthetic Communications, 2003 , vol. 33, # 10 p. 1733 - 1750
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran T=-78°C;
参考文献
Harrowven, David C.; Poon, Hon Suen
Tetrahedron Letters, 1994 , vol. 35, # 48 p. 9101 - 9102
反应条件
lithium aluminium tetrahydride in diethyl ether 4 h;
参考文献
Baumert, Miriam; Albrecht, Markus; Winkler, Henrik D. F.; Schalley, Christoph A.
Synthesis, 2010 , # 6 p. 953 - 958
反应条件
1: 91.2 percent / O2 / Co(OAc)2-Mn(OAc)2 / acetic acid / 2 h / 110 °C / 2280 Torr 2: LAH View Scheme
参考文献
Kitajima, Nobumasa; Takemura, Kazuya; Moro-Oka, Yoshihiko; Yoshikuni, Tadatsugu; Akada, Mitsuo; et al.
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 3 p. 1035 - 1038
反应条件
tetrahydrofuran; lithium aluminium tetrahydride
参考文献
Drake; Tuemmler
Journal of the American Chemical Society, 1955 , vol. 77, p. 1204,1207
反应条件
aluminum oxide; carbon dioxide; Isopulegol T=200°C; P=110207 Torr; Supercritical conditions;
参考文献
Anikeev; Sivcev; Il'Ina; Korchagina; Statsenko; Volcho; Salakhutdinov
Russian Journal of Physical Chemistry A, 2013 , vol. 87, # 3 p. 382 - 387
Kinet. Katal., 2013 , vol. 87, # 3 p. 403 - 408,6
反应条件
1: Et3N / 20 °C 2: 85 percent / sodium borohydride; LiCl / bis-(2-methoxy-ethyl) ether / 5 h / 162 °C View Scheme
参考文献
Zhu, Hua-Jie; Pittman Jr., Charles U.
Synthetic Communications, 2003 , vol. 33, # 10 p. 1733 - 1750
反应条件
1: potassium hydroxide / water / 4 h / 0 - 100 °C 2: lithium borohydride / tetrahydrofuran / 3 h / |Cooling View Scheme
参考文献
Council of Scientific and Industrial Research; Negi, Arvind Singh; Prakasham, Ayyampudur Palanisamy; Saxena, Ajit Kumar; Luqman, Suaib; Chanda, Debabrata; Kaur, Tandeep; Gupta, Atul
Patent: US2013/79396 A1, 2013 ;
反应条件
water T=90°C; pH=5; Time;
参考文献
De Nicola, Gina R.; Montaut, Sabine; Rollin, Patrick; Nyegue, Maximilienne; Menut, Chantal; Iori, Renato; Tatibouet, Arnaud
Journal of Agricultural and Food Chemistry, 2013 , vol. 61, # 1 p. 137 - 142
反应条件
oxygen; anhydrous cobalt diacetate T=110°C; P=2280 Torr; 2 h; var. catalysts; Product distribution;
参考文献
Kitajima, Nobumasa; Takemura, Kazuya; Moro-Oka, Yoshihiko; Yoshikuni, Tadatsugu; Akada, Mitsuo; et al.
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 3 p. 1035 - 1038
