3,4,5-三甲氧基苄醇合成路线 （共 102 条）
反应条件
bismuth(III) chloride; palladium diacetate; potassium carbonate T=20°C; 2 h; chemoselective reaction;
参考文献
Chemical Communications, , vol. 48, # 68 p. 8592 - 8594
反应条件
potassium phosphate; copper quinolate; tetra-(n-butyl)ammonium iodide in water; dimethyl sulfoxide T=120°C; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 78, # 19 p. 9898 - 9905
反应条件
1: copper quinolate; potassium phosphate; tetra-(n-butyl)ammonium iodide / water; dimethyl sulfoxide / 24 h / 120 °C 2: copper quinolate / water; dimethyl sulfoxide / 24 h / 120 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 19 p. 9898 - 9905
反应条件
1: SOCl2, Me2NPh 2: NaI 3: aq. HCl 4: H2SO4 View Scheme
参考文献
Cason,J.; Lynch,D.M.
Journal of Organic Chemistry, 1966 , vol. 31, p. 1883 - 1887
反应条件
phosphorus tribromide in benzene T=20°C;
参考文献
Parihar, Swati; Kumar, Amit; Chaturvedi, Amit K.; Sachan, Naresh Kumar; Luqman, Suaib; Changkija, Bendangla; Manohar, Murli; Prakash, Om; Chanda; Khan, Feroz; Chanotiya; Shanker, Karuna; Dwivedi, Anila; Konwar, Rituraj; Negi, Arvind S.
Journal of Steroid Biochemistry and Molecular Biology, 2013 , vol. 137, p. 332 - 344
反应条件
pyridine; hydrogenchloride; sodium borohydride in tetrahydrofuran; water
参考文献
Development Center for Biotechnology
Patent: US5840991 A1, 1998 ;
反应条件
1: With ammonia; iodine in water T=60°C; 2 h; 2: With ammonia; dihydrogen peroxide in water T=0 - 20°C;
参考文献
Tetrahedron Letters, , vol. 51, # 33 p. 4378 - 4381
反应条件
ammonium hydroxide; iodine T=60°C; 2 h;
参考文献
Iida, Shinpei; Togo, Hideo
Tetrahedron, 2007 , vol. 63, # 34 p. 8274 - 8281
反应条件
1: With ammonia; iodine in water T=60°C; 2 h; 2: With ammonia; dihydrogen peroxide in water T=0 - 20°C;
参考文献
Tetrahedron Letters, , vol. 51, # 33 p. 4378 - 4381
反应条件
palladium dichloride in methanol T=40°C; 24 h; Inert atmosphereGreen chemistry;
参考文献
Wang, Hu; Li, Li; Bai, Xing-Feng; Deng, Wen-Hui; Zheng, Zhan-Jiang; Yang, Ke-Fang; Xu, Li-Wen
Green Chemistry, 2013 , vol. 15, # 9 p. 2349 - 2355
