2-propyl-[1,3]dioxane; lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 0.2 h, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bonner, Trevor G.; Lewis, David; Rutter, Keith
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1807 - 1810
di-tert-butyl peroxide in chlorobenzene T=130°C; 4 h; Product distribution;
参考文献
Zorin, V. V.; Batyrbaev, N. A.; Zlot-skii, S. S.; Rakhmankulov, D. L.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 347 - 352
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 387 - 393
Bonner, Trevor G.; Lewis, David; Rutter, Keith
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1807 - 1810
2-propyl-[1,3]dioxane; lithium aluminium tetrahydride; boron trichloride
1.) CH2Cl2, 0.2 h, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bonner, Trevor G.; Lewis, David; Rutter, Keith
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1807 - 1810
