ethanol in ethylene glycol dimethyl ether; ethanol at room temp.; anal. by IR, GLC and liq. chromy.;

tetrabutyl-ammonium chloride in acetonitrile Electrolysis; electrolysis of soln. of alc., tetrabutylammonium chloride in MeCN was conducted in H-type cell using Zn plate as anode and Pt foil as cathode; potential applied - 25 V, electricity passed - 700 Coulombs; solid sepd. in the anode was filtered; washed (MeCN, dry ether); dried (vac.); elem. anal.;