2-甲基-1-丙基溴化镁合成路线 （共 44 条）
反应条件
iron (III) acetylacetonate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=80°C; 2 h;
参考文献
Rao Volla, Chandra M.; Vogel, Pierre
Angewandte Chemie - International Edition, 2008 , vol. 47, # 7 p. 1305 - 1307
反应条件
dilithium tetrachlorocuprate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=20°C; Alkylation;
参考文献
Cahiez, Gerard; Chaboche, Christophe; Jezequel, Michelle
Tetrahedron, 2000 , vol. 56, # 18 p. 2733 - 2737
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran
55 h; Heating;
参考文献
Cho, Chul-Hee; Yun, Hee-Sung; Park, Kwangyong
Journal of Organic Chemistry, 2003 , vol. 68, # 8 p. 3017 - 3025
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran
55 h; Heating;
参考文献
Cho, Chul-Hee; Yun, Hee-Sung; Park, Kwangyong
Journal of Organic Chemistry, 2003 , vol. 68, # 8 p. 3017 - 3025
反应条件
in tetrahydrofuran
5 h;
参考文献
Rao, A. V. Rama; Rao, M. Narayana; Garyali, Kamini
Synthetic Communications, 1984 , vol. 14, # 6 p. 557 - 564
反应条件
tetrahydrofuran; diethyl ether
参考文献
Bishop,D.C. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 670 - 673
反应条件
1: in tetrahydrofuran
T=-40°C; 1 h;
2: With water; ammonium chloride in tetrahydrofuran
参考文献
Barth, Francis; Congy, Christian; Guillaumont, Carole; Rinaldi, Murielle; Vasse, Fabienne; Vernhet, Claude
Patent: US2004/34090 A1, 2004 ;
Location in patent: Page/Page column 8 ;
反应条件
in diethyl ether
T=-10 - 20°C;
参考文献
Marcou,A.; Normant,H.
Bulletin de la Societe Chimique de France, 1965 , p. 3491 - 3494
反应条件
copper(I) bromide dimethylsulfide complex in N,N,N',N',N'',N''-hexamethylphosphoric triamide; dichloromethane
T=-25°C; 2 h;
参考文献
Sviridov, A. F.; Ermolenko, M. S; Yashunsky, D. V.; Kochetkov, N. K.
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4359 - 4362
反应条件
copper(I) bromide dimethylsulfide complex in N,N,N',N',N'',N''-hexamethylphosphoric triamide; dichloromethane
T=-25°C; 2 h;
参考文献
Sviridov, A. F.; Ermolenko, M. S; Yashunsky, D. V.; Kochetkov, N. K.
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4359 - 4362
