2-甲基-1,2,3,4-四氢萘合成路线 （共 32 条）
参考文献
Morin,F.G.; Horton,W.J.; Grant,D.M.
Journal of the American Chemical Society, 1983 , vol. 105, p. 3992
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
T=80°C;
参考文献
Rigollier, Pascal; Young, Jonathan R.; Fowley, Lissa A.; Stille, John R.
Journal of the American Chemical Society, 1990 , vol. 112, # 25 p. 9441 - 9442
反应条件
tetra-n-butylammonium acetate in chloroform
T=60°C; 1 h;
参考文献
Fujita, Morifumi; Kim, Wan Hyeok; Sakanishi, Yuichi; Fujiwara, Koji; Hirayama, Sayaka; Okuyama, Tadashi; Ohki, Yasuhiro; Tatsumi, Kazuyuki; Yoshioka, Yasunori
Journal of the American Chemical Society, 2004 , vol. 126, # 24 p. 7548 - 7558
反应条件
triethyl borane; tri-n-butyl-tin hydride in hexane; benzene
T=20°C; 1 h;
参考文献
Miura, Katsukiyo; Ichinose, Yoshifumi; Nozaki, Kyoko; Fugami, Keigo; Oshima, Koichiro; Utimoto, Kiitiro
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 1 p. 143 - 147
反应条件
1: 83 percent / NaBH4 / ethanol; tetrahydrofuran / 25 °C
2: 96 percent / p-toluenesulfonic acid / benzene / Heating
3: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating
4: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: p-toluenesulfonic acid / benzene / Heating
2: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating
2: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 96 percent / p-toluenesulfonic acid / benzene / Heating
2: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating
3: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: LDA
2: NaBH4 / tetrahydrofuran; methanol
3: p-toluenesulfonic acid / benzene / Heating
4: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
nickel
T=207 - 250°C; P=19858.7 - 41923.9 Torr; Hydrogenation;
参考文献
Kaliberdo et al.
Izv. Sibirsk. Otd. Akad. S.S.S.R.Chem.Abstr., 1958 , # 3 p. 77
Izv. Sibirsk. Otd. Akad. S.S.S.R.Chem.Abstr., 1959 , p. 4225
