R(+)-alpha-甲基苄胺合成路线 （共 285 条）
反应条件
(+/-)-camphoric anhydride man verseift das entstehende <d-Camphersaeure>-α-<d-α-phenaethylamid> mit siedender 30prozentiger Salzsaeure;
参考文献
Freylon
Annales de Chimie (Cachan, France), 1908 , vol. <8>15, p. 143
参考文献
BASF Aktiengesellschaft
Patent: US6720447 B1, 2004 ;
Location in patent: Page column 6 ;
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gawley, Robert E.; Rein, Kathleen; Chemburkar, Sanjay
Journal of Organic Chemistry, 1989 , vol. 54, # 13 p. 3002 - 3004
反应条件
lithium aluminium tetrahydride; 3-O-cyclohexylmethyl-1,2-O-cyclohexylidene-α-D-glucofuranose in diethyl ether 2.5 h; HeatingLiAlH4 concentration effect on enantiomeric excess; asymmetric reduction of ketones and isoelectronic ketone oximes with LiAlH4-3-O-cyclohexylmethyl-1,2-O-cyclohexylidene-α-D-glucofuranose complex; Product distribution;
参考文献
Landor, Stephen R.; Chan, Yuet M.; Sonola, Olutunji O.; Tatchell, Austin R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 493 - 496
反应条件
(1S,2R)-cis-2-aminocyclopentanol; borane in tetrahydrofuran 40 h; Ambient temperatureother chiral ligands, enantioselectivity; Product distribution;
参考文献
Didier, Eric; Loubinoux, Bernard; Ramos Tombo, Gerardo H.; Rihs, Grety
Tetrahedron, 1991 , vol. 47, # 27 p. 4941 - 4958
反应条件
oxygen; tetra-(n-butyl)ammonium iodide in ethanol T=20°C; 3 h; Electrochemical reaction;
参考文献
Zhang, Zhenlei; Su, Jihu; Zha, Zhenggen; Wang, Zhiyong
Chemical Communications, 2013 , vol. 49, # 79 p. 8982 - 8984
反应条件
dicyclohexyl-carbodiimide in dichloromethane a) -20 deg C, 2 h, b) r.t., 6 h;
参考文献
Takeuchi, Yoshio; Itoh, Noriaki; Satoh, Toshihiro; Koizumi, Toru; Yamaguchi, Kentaro
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1812 - 1820
参考文献
Harada,K.; Matsumoto,K.
Journal of Organic Chemistry, 1967 , vol. 32, p. 1794 - 1800
反应条件
1: in ethanol T=35 - 75°C; 30 h; 2: With hydrogenchloride in water; ethyl acetate 1 h;
参考文献
CADILA HEALTHCARE LIMITED; DWIVEDI, Shri Prakash Dhar; SINGH, Ramesh Chandra; CHAVDA, Rajendra Gokalbhai
Patent: WO2013/121440 A1, 2013 ;
Location in patent: Page/Page column 26; 27 ;
反应条件
1: With vinyl ethyl ketone in tetrahydrofuran T=40°C; 2: With sodium methylate T=20°C;
参考文献
Park, Ju-Young; Shin, Young-Gyun; Kim, Kee-Won; Kwon, Young-Bae; Yoon, Sung-Hwa
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 11 p. 3499 - 3502
