1-乙酰氧基-4-氯-3-甲基-2-丁烯合成路线 （共 2 条）
反应条件
N,N-dichloro-4-chlorobenzenesulfonamide; lithium perchlorate
10 h; Ambient temperature;
参考文献
Ivanov, S. V.; Stadnichuk, M. D.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 4 p. 865 - 873,763 - 769
反应条件
1: 14.8 g / CuSO4; H2SO4 / acetic acid / 96 h / 20 °C
2: 75 percent / Na2CO3; H2O / methanol / 5 h / 0 °C
3: 90 percent / pyridinium chlorochromate / CH2Cl2 / 1.5 h / 0 °C
4: 65 percent / p-toluenesulfonic acid / methanol / 18 h / 20 °C
5: 58 percent / K2HPO4; KH2PO4; NaBr / dimethylsulfoxide / 20 h / 80 °C
View Scheme
参考文献
Lambertin, Frederic; Wende, Martin; Quirin, Marie Jeanne; Taran, Martine; Delmond, Bernard
European Journal of Organic Chemistry, 1999 , # 6 p. 1489 - 1494
