2,3,4,5,6-alpha-D-葡萄糖五乙酸酯合成路线 （共 13 条）
反应条件
in [BMIm][MeHPO3] T=20°C; 15 h;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE-CNRS-
Patent: US2010/121075 A1, 2010 ;
Location in patent: Page/Page column 8 ;
反应条件
water; mercury dichloride; mercury(II) oxide in acetone 48 h; Ambient temperaturereagent, time, temperature; Product distribution;
参考文献
Miljkovic, Momcilo; Dropkin, Daniel; Hagel, Peter; Habash-Marino, Margaret
Carbohydrate Research, 1984 , vol. 128, p. 11 - 20
反应条件
1: pyridine / 4 h / Ambient temperature 2: dimethylaminopyridine / pyridine / 12 h 3: 1.) O3, 2.) dimethyl sulfide / 1.) CH2Cl2, -78 deg C, 11 h, 2.) -78 deg C to RT, 4 h View Scheme
参考文献
Weitz, David J.; Bednarski, Mark D.
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4957 - 4959
反应条件
1: dimethylaminopyridine / pyridine / 12 h 2: 1.) O3, 2.) dimethyl sulfide / 1.) CH2Cl2, -78 deg C, 11 h, 2.) -78 deg C to RT, 4 h View Scheme
参考文献
Weitz, David J.; Bednarski, Mark D.
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4957 - 4959
反应条件
1: indioside I With hydrogenchloride in 1,4-dioxane T=90°C; 2: acetic anhydride With pyridine in 1,4-dioxane T=60°C;
参考文献
Yen, Chiao-Ting; Lee, Chia-Lin; Chang, Fang-Rong; Hwang, Tsong-Long; Yen, Hsin-Fu; Chen, Chao-Jung; Chen, Shu-Li; Wu, Yang-Chang
Journal of Natural Products, 2012 , vol. 75, # 4 p. 636 - 643
反应条件
1: indioside J With hydrogenchloride in 1,4-dioxane T=90°C; 2: acetic anhydride With pyridine in 1,4-dioxane T=60°C;
参考文献
Yen, Chiao-Ting; Lee, Chia-Lin; Chang, Fang-Rong; Hwang, Tsong-Long; Yen, Hsin-Fu; Chen, Chao-Jung; Chen, Shu-Li; Wu, Yang-Chang
Journal of Natural Products, 2012 , vol. 75, # 4 p. 636 - 643
反应条件
dimethylsulfide; ozone 1.) CH2Cl2, -78 deg C, 11 h, 2.) -78 deg C to RT, 4 h; Yield given. Multistep reaction;
参考文献
Weitz, David J.; Bednarski, Mark D.
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4957 - 4959
反应条件
pyridine; β-glucosidase Multistep reaction;
参考文献
Ueda, Katsuhiro; Yasutomi, Kazuko; Mori, Iwao
Chemistry Letters, 1983 , p. 149 - 150
参考文献
Wolfrom et al.
Journal of the American Chemical Society, 1934 , vol. 56, p. 1794
参考文献
Weygand et al.
Chemische Berichte, 1958 , vol. 91, p. 1040
