4-叔-丁基-2-氟-苯酚合成路线 （共 19 条）
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in methanol 5 h; Heating;
参考文献
Zupan, Marko; Iskra, Jernej; Stavber, Stojan
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 6 p. 1655 - 1660
反应条件
N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide
T=85 - 90°C;
参考文献
Stavber, Gaj; Zupan, Marko; Stavber, Stojan
Tetrahedron Letters, 2007 , vol. 48, # 15 p. 2671 - 2673
反应条件
accufluorTM in acetonitrile
T=80°C; 1 h; Overall yield = 92 percent;
参考文献
Pravst, Igor; Stavber, Stojan
Journal of Fluorine Chemistry, 2013 , vol. 156, p. 276 - 282
反应条件
AlCl3, aluminium chloride
T=0 - 20°C;
参考文献
Astellas Pharma Inc.
Patent: EP1955697 A1, 2008 ;
Location in patent: Page/Page column 21 ;
反应条件
sulfuric acid in benzene
T=60°C; 5 h;
参考文献
Stokker; Deana; deSolms; Schultz; Smith; Cragoe Jr.; Baer; Ludden; Russo; Scriabine; Sweet; Watson
Journal of Medicinal Chemistry, 1980 , vol. 23, # 12 p. 1414 - 1427
反应条件
1: With [bis(2-methoxyethyl)amino]-sulfur trifluoride in chloroform
T=0 - 20°C; Inert atmosphere;
2: With sodium tetrahydroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene in ethanol
T=0 - 50°C;
参考文献
Nemoto, Hiroyuki; Nishiyama, Tsuyoshi; Akai, Shuji
Organic Letters, 2011 , vol. 13, # 10 p. 2714 - 2717
反应条件
CsSO4F in acetonitrile
1 h; Ambient temperature;
参考文献
Stavber; Zupan
Tetrahedron, 1992 , vol. 48, # 28 p. 5875 - 5882
反应条件
CsSO4F in acetonitrile
1 h; Ambient temperature; Yield given;
参考文献
Stavber; Zupan
Tetrahedron, 1992 , vol. 48, # 28 p. 5875 - 5882
反应条件
CsSO4F in acetonitrile
1 h; Ambient temperature;
参考文献
Stavber; Zupan
Tetrahedron, 1992 , vol. 48, # 28 p. 5875 - 5882
反应条件
CsSO4F in acetonitrile
1 h; Ambient temperature;
参考文献
Stavber; Zupan
Tetrahedron, 1992 , vol. 48, # 28 p. 5875 - 5882
