5-(溴甲基)呋喃-2-甲醛合成路线 （共 27 条）
反应条件
hydrogen bromide; lithium bromide in water; toluene
T=65°C; 48 h;
参考文献
Kumari, Nitee; Olesen, Jens Kruse; Pedersen, Christian M.; Bols, Mikael
European Journal of Organic Chemistry, 2011 , # 7 p. 1266 - 1270
反应条件
hydrogen bromide; lithium bromide in toluene
T=65°C; 3 h;
参考文献
Jadhav, Harishchandra; Pedersen, Christian Marcus; Solling, Theis; Bols, Mikael
ChemSusChem, 2011 , vol. 4, # 8 p. 1049 - 1051
反应条件
pyridinium tribromide in toluene
1 h; Heating;
参考文献
Fayet, Catherine; Gelas, Jacques
Carbohydrate Research, 1983 , vol. 122, p. 59 - 68
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 0 °C
1.2: 2 h
2.1: sulfuric acid; water / acetic acid / 7 h / Reflux
3.1: hydrogen; palladium(II) oxide hydrate / methanol / 2 h / 50 °C / 37503.8 Torr
4.1: hydrogen bromide; lithium bromide / water; toluene / 65 °C
View Scheme
参考文献
Kumari, Nitee; Olesen, Jens Kruse; Pedersen, Christian M.; Bols, Mikael
European Journal of Organic Chemistry, 2011 , # 7 p. 1266 - 1270
反应条件
1: sulfuric acid; water / acetic acid / 7 h / Reflux
2: hydrogen; palladium(II) oxide hydrate / methanol / 2 h / 50 °C / 37503.8 Torr
3: hydrogen bromide; lithium bromide / water; toluene / 65 °C
View Scheme
参考文献
Kumari, Nitee; Olesen, Jens Kruse; Pedersen, Christian M.; Bols, Mikael
European Journal of Organic Chemistry, 2011 , # 7 p. 1266 - 1270
反应条件
sulfuric acid; water; magnesium bromide
Multistep reaction;
参考文献
Hamada, Kazuhiko; Yoshihara, Hiroshi; Suzukamo, Gohfu
Chemistry Letters, 1982 , p. 617 - 618
参考文献
Middendorp
Recueil des Travaux Chimiques des Pays-Bas, 1919 , vol. 38, p. 42
