triethylamine in diethyl ether
2 h; Ambient temperature;
参考文献
Kam, Sheung-Tsam; Matier, William L.; Mai, Khuong X.; Barcelon-Yang, Cynthia; Borgman, Robert J.; et al.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 8 p. 1007 - 1016
1: 96.2 percent / Et3N / diethyl ether / 2 h / Ambient temperature
2: dimethylformamide / 6 h / 65 °C
View Scheme
参考文献
Kam, Sheung-Tsam; Matier, William L.; Mai, Khuong X.; Barcelon-Yang, Cynthia; Borgman, Robert J.; et al.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 8 p. 1007 - 1016
1: 4-(pivaloyloxy)-iodobenzene With isopropylmagnesium chloride in tetrahydrofuran
T=-20°C; 0.5 h;
2: in tetrahydrofuran
T=-20°C;
3: 2-fluoro-benzoyl chloride in tetrahydrofuran
T=-10°C;
