4-甲氧基苯-1,2-二醇合成路线 （共 26 条）
反应条件
1: in dichloromethane
T=0 - 20°C; 66 h;
2: With lithium aluminium tetrahydride in tetrahydrofuran
T=0°C; 1 h; Further stages.;
参考文献
Tada, Masahiro; Ishiguro, Risa; Izumi, Ryohei
Chemical and Pharmaceutical Bulletin, 2008 , vol. 56, # 3 p. 239 - 242
反应条件
1: With Pd(OPiv)2; [bis(acetoxy)iodo]benzene in toluene
T=100°C; Inert atmosphere;
2: With tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C;
3: With water in tetrahydrofuran
参考文献
Huang, Chunhui; Ghavtadze, Nugzar; Chattopadhyay, Buddhadeb; Gevorgyan, Vladimir
Journal of the American Chemical Society, 2011 , vol. 133, # 44 p. 17630 - 17633
反应条件
[((2-pyridyl)bis(3-tert-butylpyrazol-2-yl)methane)Cu2O2](SbF6)2 in dichloromethane
T=-78°C; 0.166667 h; Inert atmosphere;
参考文献
Hoffmann, Alexander; Citek, Cooper; Binder, Stephan; Goos, Arne; Ruebhausen, Michael; Troeppner, Oliver; Ivanovic-Burmazovic, Ivana; Wasinger, Erik C.; Stack, T. Daniel P.; Herres-Pawlis, Sonja
Angewandte Chemie - International Edition, 2013 , vol. 52, # 20 p. 5398 - 5401
Angew. Chem., 2013 , vol. 125, # 20 p. 5508 - 5512,5
反应条件
sodium percarbonate in tetrahydrofuran; water; N,N-dimethyl-formamide
7 h; ultrasonication;
参考文献
Kabalka, G. W.; Reddy, N. K.; Narayana, C.
Tetrahedron Letters, 1992 , vol. 33, # 7 p. 865 - 866
反应条件
nitrophenol oxygenase in phosphate buffer
T=20°C; Decomposition; pH=7.5; Enzymatic reaction; Enzyme kinetics; Further Variations:Reagents;
参考文献
Folsom, Brian R.; Stierli, Ruth; Schwarzenbach, Rene P.; Zeyer, Josef
Environmental Science & Technology, 1994 , vol. 28, # 2 p. 306 - 311
反应条件
1: With C42H45N9*2Cu(2+)*O2(2-) in acetone
T=-90 - -60°C;
2: in acetone
Acidic conditions;
参考文献
Garcia-Bosch, Isaac; Ribas, Xavi; Costas, Miquel
Chemistry - A European Journal, 2012 , vol. 18, # 7 p. 2113 - 2122
反应条件
sodium peroxynitrite in phosphate buffer
T=20 - 25°C; Nitration; hydroxylation; pH=7.0; Kinetics; Further Variations:Solvents;
参考文献
Nonoyama, Nobuaki; Chiba, Kazuhiko; Hisatome, Kaori; Suzuki, Hitomi; Shintani, Futoshi
Tetrahedron Letters, 1999 , vol. 40, # 38 p. 6933 - 6937
参考文献
Hargreaves et al.
Journal of Applied Chemistry, 1958 , vol. 8, p. 273,280
反应条件
1: H2SO4
2: palladium/charcoal; methanol / Hydrogenation.anschliessendes Diazotieren und Erwaermen der Diazoniumsalz-Loesung mit CuSO4
3: aqueous NaOH
View Scheme
参考文献
Hargreaves et al.
Journal of Applied Chemistry, 1958 , vol. 8, p. 273,280
反应条件
1: palladium/charcoal; methanol / Hydrogenation.anschliessendes Diazotieren und Erwaermen der Diazoniumsalz-Loesung mit CuSO4
2: aqueous NaOH
View Scheme
参考文献
Hargreaves et al.
Journal of Applied Chemistry, 1958 , vol. 8, p. 273,280
