3,6-二氯苯-1,2-二醇合成路线 (共 7 条)
反应条件
dihydrogen peroxide in acetonitrile
T=50°C; hydroxylation; 4 h; UV-irradiation;
参考文献
Kirsch, Nils H.; Stan, H.-J.
Chemosphere, 1994 , vol. 28, # 1 p. 131 - 138
反应条件
in methanol
2 h; Heating;
参考文献
Guirado, Antonio; Cerezo, Alfredo; Lopez-Sanchez, Jose I.; Saez-Ayala, Magali; Bautista, Delia
Tetrahedron Letters, 2006 , vol. 47, # 43 p. 7583 - 7585
反应条件
in ethanol
2 h; Heating;
参考文献
Guirado, Antonio; Cerezo, Alfredo; Lopez-Sanchez, Jose I.; Saez-Ayala, Magali; Bautista, Delia
Tetrahedron Letters, 2006 , vol. 47, # 43 p. 7583 - 7585
反应条件
copper dichloride in N,N-dimethyl-formamide
参考文献
Paquet, Jacques; Brassard, Paul
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1354 - 1358
反应条件
sodium hydroxide
1.) 20 deg C, 15 min., 20 deg C, 15 min.; Yield given. Multistep reaction;
参考文献
Knuutinen, Juha S.; Tarhanen, Juhani T.
Journal of Chemical and Engineering Data, 1981 , vol. 26, # 3 p. 347
反应条件
potassium hydroxide
4 h; Ambient temperature;
参考文献
Singh, Sudhir K.; Kumar, Subodh
Journal of Agricultural and Food Chemistry, 1993 , vol. 41, # 9 p. 1511 - 1516
参考文献
Knuutinen, J.; Korhonen, I. O. O.
Organic Mass Spectrometry, 1987 , vol. 22, p. 70 - 74