反应条件
1: 1.) Li, FeCl3, NH3 / 1.) THF, r.t., 1.5 h, 2.) THF, 1 h
2: 93 percent / H2, quinoline / Pd-BaSO4 / hexane / 2 h / 0 °C
3: 1.) n-BuLi / 1.) <Rh(dppe)COD>ClO4 / 1.) THF, hexane, reflux, 6 h, 2.) THF, hexane
View Scheme
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
