5,5′,6,6′,7,7′,8,8′-八氢-1,1′-联-2-萘酚合成路线 （共 6 条）
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; air; hydrogen in isopropyl alcohol T=20°C; P=38002.6 Torr; 16 h; Molecular sieve;
参考文献
Wang, Da-Wei; Lu, Sheng-Mei; Zhou, Yong-Gui
Tetrahedron Letters, 2009 , vol. 50, # 12 p. 1282 - 1285
反应条件
5-palladium/activated carbon; hydrogen in ethanol; water T=70°C; P=36201.3 Torr; 6 h;
参考文献
Ding, Qian Chang; Du, Yun Feng; Li, Xin Sheng; Xu, Dong Cheng
Chinese Chemical Letters, 2010 , vol. 21, # 11 p. 1277 - 1280
反应条件
Fmoc-L-Asn(Trt)-L-Asn(Trt)-NH(CH2)6CONH(CH2)3-silica gel in hexane; chloroform
参考文献
Sun, Ping; Wang, Chunlei; Breitbach, Zachary S.; Zhang, Ying; Armstrong, Daniel W.
Analytical Chemistry, 2009 , vol. 81, # 24 p. 10215 - 10226
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Kazlauskas, Romas J.
Journal of the American Chemical Society, 1989 , vol. 111, # 13 p. 4953 - 4959
反应条件
sodium hydroxide; Raney Ni-Al alloy T=90°C; 6 h; Title compound not separated from byproducts;
参考文献
Guo; Ding
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 10061 - 10064
反应条件
1: morpholine; formaldehyd T=60°C; 13 h; Cooling with ice; 2: (S)-2,2'-dihydroxy-5,5',6,6',7,7',8,8'-octahydro-1,1'-binaphthyl in 1,4-dioxane T=60°C; 18 h; Inert atmosphere;
参考文献
Turlington, Mark; Pu, Lin; Kimmel, Kyle L.; Ellman, Jonathan A.
Organic Syntheses, 2010 , vol. 87, p. 59 - 67
