2-甲基-5-苯基-噁唑合成路线 （共 39 条）
参考文献
Pale-Grosdemange, Catherine; Chuche, Josselin
Tetrahedron, 1989 , vol. 45, # 11 p. 3397 - 3414
反应条件
1: 65 percent / I2 / CH2Cl2 / 2.5 h / 20 °C
2: 21 percent / K2CO3; N,N'-dimethylethylenediamine; CuI / toluene / 45 h / 110 °C
View Scheme
参考文献
Schuh, Kerstin; Glorius, Frank
Synthesis, 2007 , # 15 p. 2297 - 2306
反应条件
1: 22 percent / K2CO3; N,N'-dimethylethylenediamine; CuI / toluene / 21 h / 40 - 110 °C
2: 93 percent / K2CO3; N,N'-dimethylethylenediamine; CuI / toluene / 20 h / 110 °C
View Scheme
参考文献
Schuh, Kerstin; Glorius, Frank
Synthesis, 2007 , # 15 p. 2297 - 2306
反应条件
8-methylquinoline 1-oxide; Au(Ph3P)+NTf2-
T=60°C; 3 h;
参考文献
Wu, Chao; Liang, Zhi-Wu; Xu, Ying-Ying; He, Wei-Min; Xiang, Jian-Nan
Chinese Chemical Letters, 2013 , vol. 24, # 12 p. 1064 - 1066
反应条件
sodium hydride in ethylene glycol dimethyl ether; dimethyl sulfoxide
参考文献
Houwing,H.A. et al.
Tetrahedron Letters, 1976 , p. 143 - 146
反应条件
in acetic acid; acetonitrile
1 h; Ambient temperature;
参考文献
Kotani, Eiichi; Kobayashi, Shigeki; Adachi, Mayumi; Tsujioka, Toshiyuki; Nakamura, Kouji; Tobinaga, Seisho
Chemical & Pharmaceutical Bulletin, 1989 , vol. 37, # 3 p. 606 - 609
反应条件
chloroform; tris-(2-chloro-ethyl)-amine; sulfuric acid
参考文献
Fusco; Rossi
Gazzetta Chimica Italiana, 1951 , vol. 81, p. 511,521
反应条件
aluminium trichloride in dichloromethane
T=25°C; 0.333333 h; Product distribution;
参考文献
Doyle, Michael P.; Buhro, William E.; Davidson, James G.; Elliott, Robert C.; Hoekstra, James W.; Oppenhuizen, Mark
Journal of Organic Chemistry, 1980 , vol. 45, # 18 p. 3657 - 3664
反应条件
1: benzene / 2 h / Reflux
2: acetonitrile / Flash photolysis; Inert atmosphere
3: methanol / Inert atmosphere
View Scheme
参考文献
Rajam, Sridhar; Murthy, Rajesh S.; Jadhav, Abhijit V.; Li, Qian; Keller, Christopher; Carra, Claudio; Pace, Tamara C.S.; Bohne, Cornelia; Ault, Bruce S.; Gudmundsdottir, Anna D.
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9934 - 9945
反应条件
1: acetonitrile / Flash photolysis; Inert atmosphere
2: methanol / Inert atmosphere
View Scheme
参考文献
Rajam, Sridhar; Murthy, Rajesh S.; Jadhav, Abhijit V.; Li, Qian; Keller, Christopher; Carra, Claudio; Pace, Tamara C.S.; Bohne, Cornelia; Ault, Bruce S.; Gudmundsdottir, Anna D.
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9934 - 9945
