palladium diacetate; sodium hexamethyldisilazane; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine in toluene T=20°C; 15 h; Title compound not separated from byproducts.;
参考文献
Moradi; Buchwald
Journal of the American Chemical Society, 2001 , vol. 123, # 33 p. 7996 - 8002
1: 1-bromo-4-(1,1-dimethylethyl)benzene With n-butyllithium in tetrahydrofuran T=-78°C; 0.5 h; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran T=-78°C; Further stages.;
参考文献
Molecular Crystals and Liquid Crystals, , vol. 471, # 1 p. 89 - 98
1: With sodium hydrogencarbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide T=150°C; Heck reaction; 20 h; 2: With hydrogenchloride in tetrahydrofuran T=25°C; Further stages.;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
