1,4-二硫-2,5-二醇合成路线 （共 39 条）
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=10°C; 2 h;
参考文献
UBE INDUSTRIES, LTD.
Patent: WO2006/123648 A1, 2006 ;
Location in patent: Page/Page column 14 ;
反应条件
triethylamine in 1,4-dioxane
参考文献
Nagaoka, Hitoshi; Hara, Hiromu; Mase, Toshiyasu
Heterocycles, 1990 , vol. 31, # 7 p. 1241 - 1244
反应条件
1: in ethanol T=20°C; 0.166667 h; 2: With N-methylpiperazine-functionalized Polyacrylonitrile Fiber in ethanol Gewald Aminoheterocycles Synthesis; 4 h; Reflux;
参考文献
Ma, Lichao; Yuan, Liwei; Xu, Changzhu; Li, Guowei; Tao, Minli; Zhang, Wenqin
Synthesis (Germany), 2013 , vol. 45, # 1 art. no. SS-2012-H0716-OP, p. 45 - 52
反应条件
acetic acid in ethanol Heating;
参考文献
Barry,V.C. et al.
Journal of Medicinal Chemistry, 1970 , vol. 13, p. 421 - 427
反应条件
propan-1-ol; ammonia anschliessend Behandeln mit FeCl3 in Aethanol;
参考文献
Thiel et al.
Justus Liebigs Annalen der Chemie, 1958 , vol. 611, p. 131,137
反应条件
lithium bromide in 1,4-dioxane 20 h; Reflux;
参考文献
Tetrahedron, , vol. 67, # 45 p. 8679 - 8684
反应条件
1: With 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran; 1,2-dichloro-ethane T=50 - 67°C; 3 h; 2: With hydrogenchloride in tetrahydrofuran; water; 1,2-dichloro-ethane T=60°C; 2.5 h; Product distribution / selectivity;
参考文献
UBE INDUSTRIES, LTD.
Patent: WO2006/123648 A1, 2006 ;
Location in patent: Page/Page column 27-28 ;
反应条件
titanium tetrachloride in 1,2-dichloro-ethane T=67 - 80°C; 5 - 7 h; Product distribution / selectivity;
参考文献
UBE INDUSTRIES, LTD.
Patent: WO2006/123648 A1, 2006 ;
Location in patent: Page/Page column 20-21 ;
参考文献
Hromatka; Haberl
Monatshefte fuer Chemie, 1954 , vol. 85, p. 1088,1094
反应条件
triethylamine in ethanol T=20°C; 2.08333 h; Heating / reflux;
参考文献
Smithkline Beecham Corporation
Patent: WO2003/104218 A1, 2003 ;
Location in patent: Page 13 ;
WO 03/104218 A1
