3-(4,5-二氢-2-噁唑)吡啶合成路线 (共 9 条)
反应条件
bismuth trifluoromethanesulphonate 4 h; Heating;
参考文献
Mirkhani, Valiollah; Moghadam, Majid; Tangestaninejad, Shahram; Mohammadpoor-Baltork, Iraj; Mahdavi, Mohammad
Monatshefte fur Chemie, 2009 , vol. 140, # 12 p. 1489 - 1494
反应条件
sodium hydride in ethylene glycol dimethyl ether T=20 - 40°C; 29 h;
参考文献
Ikeda, Katsuya; Honda, Hiroyuki; Matsuo, Takanori; Yamamoto, Tamotsu
Organic Preparations and Procedures International, 1995 , vol. 27, # 1 p. 103 - 106
反应条件
1: 3 - 4 h; Heating; 2: With boric acid in toluene T=130°C; 3: With CaO T=280°C; 3 h;
参考文献
Ilkgul, Baris; Gunes, Deniz; Sirkecioglu, Okan; Bicak, Niyazi
Tetrahedron Letters, 2010 , vol. 51, # 40 p. 5313 - 5315
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride in toluene 2 h; RefluxInert atmosphere;
参考文献
Boissarie, Patrick J.; Hamilton, Zoe E.; Lang, Stuart; Murphy, John A.; Suckling, Colin J.
Organic Letters, 2011 , vol. 13, # 23 p. 6256 - 6259
反应条件
palladium diacetate; magnesium sulfate; triethylamine; di-(1-adamantyl)-n-butylphosphine in toluene T=110°C; P=7500.75 Torr; 16 h; AutoclaveInert atmosphere;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Neumann, Stephan; Beller, Matthias
Chemistry - A European Journal, 2012 , vol. 18, # 43 p. 13619 - 13623
反应条件
1: 0.75 h / 80 °C 2: potassium carbonate / water / 6 h / 80 °C View Scheme
参考文献
Goud, D. Raghavender; Pathak, Uma
Synthesis (Germany), 2012 , vol. 44, # 23 art. no. SS-2012-Z0598-OP, p. 3678 - 3682
反应条件
in sodium hydroxide T=60°C; 5 h;
参考文献
Nagai; Kikuchi; Nagano; Shiba
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 3 p. 1063 - 1070
参考文献
Drefahl; Koenig
Chemische Berichte, 1954 , vol. 87, p. 1632
Full Text Show Details
Bras; Skorodumow
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 770,772, 773; engl. Ausg. S. 881
反应条件
hydrogenchloride; diethyl ether; ethanol
参考文献
Bras; Skorodumow
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 770,772, 773; engl. Ausg. S. 881