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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-甲酰基苯硼酸
合成路线
（共 110 条）
2178-24-7
Alpha-溴苯乙酸乙酯
+
40138-16-7
2-甲酰基苯硼酸
→
反应条件
4895-92-5
9-菲羧酸乙酯
反应条件
caesium carbonate; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine; tetrakis(triphenylphosphine) palladium(0) in ethanol; toluene T=120 - 150°C; 0.166667 h; microwave irradiation;
参考文献
Young, Ha Kim; Lee, Hyuk; Yeong, Joon Kim; Bum, Tae Kim; Heo, Jung-Nyoung
Journal of Organic Chemistry, 2008 , vol. 73, # 2 p. 495 - 501
1042722-42-8
+
40138-16-7
2-甲酰基苯硼酸
→
反应条件
53948-09-7
马兜铃内酰胺 BII
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in ethanol; toluene T=150°C; Suzuki-Miyaura coupling /aldol condensation reaction; P=4500.45 - 6000.6 Torr; 0.166667 h; Microwave irradiationInert atmosphere;
参考文献
Choi, Young Lok; Kim, Joa Kyum; Choi, Sang-Un; Min, Yong-Ki; Bae, Myung-Ae; Kim, Bum Tae; Heo, Jung-Nyoung
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 11 p. 3036 - 3040
40138-16-7
2-甲酰基苯硼酸
→
反应条件
57932-07-7
反应条件
1: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran; water / 8 h / 80 °C 2: toluene-4-sulfonic acid / benzene / 7 h / |Reflux 3: Grubb's 2nd generation catalyst / dichloromethane / 11.5 h / 20 °C 4: 2-mesityl-2,5,6,7-tetrahydropyrrolo[2,1-c][1,2,4]triazol-4-ium chloride; triethylamine / toluene / 80 °C View Scheme
参考文献
Youn, So Won; Song, Hyoung Sub; Park, Jong Hyub
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 15 p. 2388 - 2393
15952-61-1
6-氯-3,4-亚甲基二氧苯甲醛
+
40138-16-7
2-甲酰基苯硼酸
→
反应条件
61440-93-5
反应条件
tris-(dibenzylideneacetone)dipalladium(0); KF*2H2O; [(t-Bu)3PH]BF4 in tetrahydrofuran Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Xia, Ying; Liu, Zhenxing; Xiao, Qing; Qu, Peiyuan; Ge, Rui; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5714 - 5717
4784-77-4
1-溴-2-丁烯
+
40138-16-7
2-甲酰基苯硼酸
→
反应条件
62708-42-3
(9ci)-2-(2-丙烯基)-苯甲醛
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium carbonate in tetrahydrofuran; water T=80°C; 8 h;
参考文献
Youn, So Won; Song, Hyoung Sub; Park, Jong Hyub
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 15 p. 2388 - 2393
40138-16-7
2-甲酰基苯硼酸
+
106-95-6
3-溴丙烯
→
反应条件
62708-42-3
(9ci)-2-(2-丙烯基)-苯甲醛
反应条件
potassium phosphate; bis(benzonitrile)palladium(II) dichloride in N,N-dimethyl acetamide; water Suzuki-Miyaura Coupling;
参考文献
Cera, Gianpiero; Chiarucci, Michel; Dosi, Federico; Bandini, Marco
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 11-12 p. 2227 - 2231
6298-19-7
3-氨基-2-氯吡啶
+
40138-16-7
2-甲酰基苯硼酸
→
反应条件
3875-08-9
反应条件
sodium carbonate; palladium diacetate; triphenylphosphine in dimethyl-ether; water 24 h;
参考文献
INDUSTRIAL TECHNOLOGY RESEARCH INSTITUTE
Patent: US2008/214818 A1, 2008 ;
Location in patent: Page/Page column 4 ;
40138-16-7
2-甲酰基苯硼酸
+
159898-15-4
1-溴-9h-吡啶并[3,4-b]吲哚
→
反应条件
38478-71-6
反应条件
1: With tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; ethanol T=20°C; Suzuki Coupling; 0.166667 h; Inert atmosphereSealed tube; 2: With sodium carbonate in ethylene glycol dimethyl ether; ethanol; water T=90°C; 0.25 h; Inert atmosphereSealed tubeMicrowave irradiation;
参考文献
Gehring, Andre P.; Tremmel, Tim; Bracher, Franz
Synthesis (Germany), 2014 , vol. 46, # 7 art. no. 1931, p. 893 - 898
40138-16-7
2-甲酰基苯硼酸
+
501-65-5
二苯基乙炔
→
反应条件
53347-50-5
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2 in 1,4-dioxane; water T=60°C; 4 h;
参考文献
Shintani, Ryo; Okamoto, Kazuhiro; Hayashi, Tamio
Chemistry Letters, 2005 , vol. 34, # 9 art. no. CL-050872, p. 1294 - 1295
87199-16-4
3-甲酰基苯硼酸
+
40138-16-7
2-甲酰基苯硼酸
+
100-39-0
溴化苄
→
反应条件
52315-08-9
3-苄基苯甲醛
反应条件
potassium carbonate; Pd(PPh3)4 in tetrahydrofuran
参考文献
The Regents of the University of California
Patent: US2003/149038 A1, 2003 ;
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