3-苯基-1,1'-联(环己基)合成路线 （共 15 条）
反应条件
MCM-22/alumina
T=130°C; P=111433 Torr; 45.6 h; Product distribution / selectivity;
参考文献
EXXONMOBIL CHEMICAL PATENTS INC.; DAKKA, Jihad, M.; XU, Teng; LEMON, Edward, A.; LATTNER, James, R.; CHENG, Jane, C.
Patent: WO2012/87433 A1, 2012 ;
Location in patent: Page/Page column 14-17 ;
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
参考文献
Blackwell,J.; Hickinbottom,W.J.
Journal of the Chemical Society, 1963 , p. 518 - 523
反应条件
1: oxalic acid
2: H2 / Pd-C / ethyl acetate
View Scheme
参考文献
Blackwell,J.; Hickinbottom,W.J.
Journal of the Chemical Society, 1963 , p. 518 - 523
反应条件
2: oxalic acid
3: H2 / Pd-C / ethyl acetate
View Scheme
参考文献
Blackwell,J.; Hickinbottom,W.J.
Journal of the Chemical Society, 1963 , p. 518 - 523
反应条件
pyridine hydrochloride
T=230°C; 6 h;
参考文献
Giannangeli, M.; Baiocchi, L.
Tetrahedron, 1980 , vol. 36, p. 1381 - 1384
反应条件
1: NaBH4 / methanol / Ambient temperature
2: 0.5 g / pyridine hydrochloride (PyHCl) / 6 h / 230 °C
View Scheme
参考文献
Giannangeli, M.; Baiocchi, L.
Tetrahedron, 1980 , vol. 36, p. 1381 - 1384
参考文献
Tamao,K. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 1958 - 1969
反应条件
1: AlCl3
2: AlCl3
View Scheme
参考文献
Nametkin; Pokrowsskaja
Zhurnal Obshchei Khimii, 1937 , vol. 7, p. 962,970
Chem. Zentralbl., 1937 , vol. 108, # II p. 1569
反应条件
aluminium trichloride
参考文献
Nametkin; Pokrowsskaja
Zhurnal Obshchei Khimii, 1937 , vol. 7, p. 962,970
Chem. Zentralbl., 1937 , vol. 108, # II p. 1569
参考文献
Turowa-Poljak; Dawydowa
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 2710,2713; engl. Ausg. S. 3019, 3021
