1: 20 percent / Na2CO3 / ethanol; H2O / 2.5 h / Ambient temperature
2: 1.7 g / SOCl2, DMF / 2 h / Heating
View Scheme
参考文献
Talekar, D. G.; Joshi, P. L.; Ramaiah, P.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 145 - 151
Talekar, D. G.; Joshi, P. L.; Ramaiah, P.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 145 - 151
chlorine in neat (no solvent)
Ambient temperaturechlorine substitution on the alcoholic chain of aliphatic C2-C8 n-alkyl acetates, chloroacetates, dichloroacetates and trichloroacetates; formation of monochloro isomers; Product distribution;
参考文献
Kophornen, Ilpo O. O.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 10 p. 721 - 724
