3,4-二甲氧基苯基乙醛酸乙酯合成路线 （共 11 条）
反应条件
sulfuric acid; palladium; acetic acid weiteres Reagens: Bromwasserstoff;
参考文献
Kindler; Metzendorf; Kwok
Chemische Berichte, 1943 , vol. 76, p. 308,314
参考文献
Kindler; Metzendorf; Dschi-yin-Kwok
Chemische Berichte, 1943 , vol. 76, p. 308,313
反应条件
boron triethoxide; (1R,2R,4aS,7R,8aR,9aS)-2-isopropenyl-1-isopropyl-4,4,7-trimethyldecahydro-9-oxa-3a-azacyclopenta[b]naphthalen-1-ol in toluene T=-35°C; 90.5 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Infante, Rebeca; Nieto, Javier; Andres, Celia
Chemistry - A European Journal, 2012 , vol. 18, # 14 p. 4375 - 4379
反应条件
(S)-Ph(OH)CCONHBn in toluene T=0°C; 4 h; Title compound not separated from byproducts;
参考文献
Blay, Gonzalo; Fernandez, Isabel; Marco-Aleixandre, Alicia; Pedro, Jose R.
Synthesis, 2007 , # 23 p. 3754 - 3757
反应条件
sodium tetrahydroborate in ethanol T=-30°C; 0.25 h;
参考文献
Ianni, Alen; Waldvogel, Siegfried R.
Synthesis, 2006 , # 13 p. 2103 - 2112
参考文献
Kindler; Metzendorf; Dschi-yin-Kwok
Chemische Berichte, 1943 , vol. 76, p. 308,313
反应条件
aluminium trichloride in dichloromethane
T=20°C; Friedel-Crafts acylation; 1 h;
参考文献
Ianni, Alen; Waldvogel, Siegfried R.
Synthesis, 2006 , # 13 p. 2103 - 2112
参考文献
Ciba Specialty Chemicals Corporation
Patent: US6596445 B1, 2003 ;
反应条件
in tetrahydrofuran
T=-78°C; 1 h; Inert atmosphere;
参考文献
Infante, Rebeca; Nieto, Javier; Andres, Celia
Chemistry - A European Journal, 2012 , vol. 18, # 14 p. 4375 - 4379
参考文献
Kindler; Metzendorf; Dschi-yin-Kwok
Chemische Berichte, 1943 , vol. 76, p. 308,313
