(2-甲酰基苯氧基)乙酸甲酯合成路线 (共 8 条)
反应条件
triethylamine in dichloromethane T=20°C; 6 h; Inert atmosphere; chemoselective reaction;
参考文献
Augustine, John Kallikat; Bombrun, Agnes; Venkatachaliah, Srinivasa; Jothi, Anandh
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 46 p. 8065 - 8072
反应条件
alum in neat (no solvent) T=80°C; 12 h; Green chemistry;
参考文献
Shunmugadhas, Ganesan; Kumar, Suresh; Kumaresan, Sudalaiandi
Journal of Chemical Sciences (Bangalore), 2012 , vol. 124, # 4 p. 857 - 863,7
反应条件
potassium carbonate in N-methyl-acetamide
参考文献
Advanced Therapies, Inc.
Patent: US5364880 A1, 1994 ;
反应条件
potassium carbonate in ethanol Etherification; 15 h; Heating;
参考文献
Desai; Dave; Shah; Vyas
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 4 p. 277 - 282
反应条件
1: aqueous NaOH 2: hydrochloric acid View Scheme
参考文献
Cajar
Chemische Berichte, 1898 , vol. 31, p. 2809
反应条件
potassium hydroxide in methanol
参考文献
Hullar,T.L.; Failla,D.L.
Journal of Medicinal Chemistry, 1969 , vol. 12, # 3 p. 420 - 424
反应条件
n-dodecyltriphenylphosphonium bromide; sodium hydride; dimethyl sulfoxide 2 h; Ambient temperature;
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 3144 - 3177
反应条件
1: KOH / methanol
2: NaBH4, aq. NaOH
View Scheme
参考文献
Hullar,T.L.; Failla,D.L.
Journal of Medicinal Chemistry, 1969 , vol. 12, # 3 p. 420 - 424