2-(2-氧代环己基)丙二酸二乙酯合成路线 （共 12 条）
反应条件
sodium hydride in benzene 5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 45, # 1 p. 43 - 47
反应条件
sodium hydride in tetrahydrofuran T=10 - 15°C; 0.0833333 h;
参考文献
Tetrahedron, , vol. 47, # 42 p. 8883 - 8906
反应条件
1: With chloro-trimethyl-silane; iron; acetic acid in tetrahydrofuran T=20°C; 0.5 h; 2: With water in tetrahydrofuran T=20°C; 0.25 h;
参考文献
Tetrahedron Letters, , vol. 51, # 27 p. 3555 - 3557
反应条件
triethyl borane; oxygen in tetrahydrofuran T=20°C;
参考文献
Chemical Communications, , # 27 p. 2893 - 2895
反应条件
sodium hydride in benzene 3.5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 45, # 1 p. 43 - 47
反应条件
1: 1) Na / 1. benzene, reflux, 8 h; 2. 2h at 0 deg C, then 6 h room temp. 2: 85 percent / NaH / benzene / 5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 1 p. 43 - 47
反应条件
1: 70 percent / 15percent H2O2, 2N NaOH / methanol 2: 62 percent / NaH / tetrahydrofuran / 0.08 h / 10 - 15 °C View Scheme
参考文献
Tetrahedron, , vol. 47, # 42 p. 8883 - 8906
反应条件
1: 84 percent / Et3N / tetrahydrofuran / 1 h / Heating; Irradiation 2: 96 percent / KF / acetone / 1 h / Ambient temperature View Scheme
参考文献
Chemische Berichte, , vol. 119, # 2 p. 444 - 452
反应条件
1: 84 percent / Et3N / tetrahydrofuran / 1 h / Heating; Irradiation 2: 96 percent / KF / acetone / 1 h / Ambient temperature View Scheme
参考文献
Chemische Berichte, , vol. 119, # 2 p. 444 - 452
反应条件
in N,N-dimethyl-formamide T=20°C; electrochemical reaction: 0.1 mol/dm3 Et4NClO4, mercury pool cathode, -2,0 V;
参考文献
Bulletin de la Societe Chimique de France, , vol. 130, p. 712 - 719
