4-硝基-N-苯基邻苯二甲酰亚胺合成路线 (共 7 条)
反应条件
acetic acid 3 h; Heating;
参考文献
Bailleux; Vallee; Nuyts; Vamecq
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 9 p. 1817 - 1821
反应条件
[bis(acetoxy)iodo]benzene T=140°C; 4 h;
参考文献
Kim, Hyun Jin; Kim, Jiyu; Cho, Seung Hwan; Chang, Sukbok
Journal of the American Chemical Society, 2011 , vol. 133, # 41 p. 16382 - 16385
反应条件
1: 88 percent / acetic anhydride / 0.33 h / Heating 2: 95 percent / acetic acid / 3 h / Heating View Scheme
参考文献
Bailleux; Vallee; Nuyts; Vamecq
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 9 p. 1817 - 1821
反应条件
in N,N-dimethyl-formamide T=70 - 100°C; 3.5 h;
参考文献
Nosova, G. I.; Koton, M. M.; Mikhailova, N. V.; Lyubimova, G. V.; Denisov, V. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 8 p. 1677 - 1680
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 8 p. 1810 - 1813
反应条件
sodium sulfide in N,N-dimethyl-formamide
参考文献
General Electric Company
Patent: US4054584 A1, 1977 ;
反应条件
in N,N-dimethyl-formamide
2 h; water bath;
参考文献
Derkacheva, V. M.; Luk'yanets, E. A.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 10 p. 2313 - 2318,1874 - 1878
反应条件
sodium hydroxide in water; acetic acid; dimethyl sulfoxide; toluene
参考文献
General Electric Company
Patent: US3957862 A1, 1976 ;