sulfuric acid; water in benzene

hydroxylamine; acetic acid

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<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '4122952', constants.ctx, '0')">sodium hydride</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=0&deg;C;&nbsp;<br /> &nbsp;

Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '605351', constants.ctx, '0')">ethyl vinyl ether</a> <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3602276', constants.ctx, '0')">palladium diacetate</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a> <br /> <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '471389', constants.ctx, '0')">benzoyl chloride</a> T=80&deg;C;&nbsp;Heck reaction;&nbsp;24&nbsp;h;&nbsp;<br /> &nbsp;

&nbsp;(i) NaOMe, (ii) /BRN= 1209224/;&nbsp;&nbsp;Multistep reaction;&nbsp;<br /> &nbsp;